PROCESS OPTIMIZATION OF CL-20 PREPARATION

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BAYAT Y.; ABRISHAMI F.; DEHGHANI H.

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Journal: JOURNAL OF ENERGETIC MATERIALS Year:2008 | Volume:2 | Issue:2 Page(s): 3-14

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Information Journal Paper

Title

PROCESS OPTIMIZATION OF CL-20 PREPARATION

Author(s)

BAYAT Y. | ABRISHAMI F. | DEHGHANI H. | Issue Writer Certificate

Keywords

ENERGETIC MATERIALSQ4

CAGED NITRAMINE EXPLOSIVESQ4

HEXANITROHEXAAZAISOWURTZITANE (CLQ4

20)Q3

NITRATIONQ3

Abstract

The caged polynitramine explosive (CL-20) is one of the most powerful explosives whose performance parameters such as pressure and velocity of detonation, heat of formation, penetration and density are higher than the other common explosives. In this paper, all the synthetic methods and the explosion parameters of CL-20 have been reviewed and the most convenient method has been selected, clarified and optimized. Also, optimizing parameters such as crystallization solvents for CL-20 (ethyl acetate-heptane) and its intermediates (for HBIW, ethyl acetate), reaction temperature (for converting HBIW to TADB, 38-42oC), and catalyst (Pd/C, 5% wet), a new nitration composition (nitric acid-sulforic acid, with ratio 1:1) has been introduced.

Cites

IMPROVEMENT OF THE PRODUCTION EFFICIENCY OF HBIW USING NEW CATALYSTS

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APA: Copy

BAYAT, Y., ABRISHAMI, F., & DEHGHANI, H.. (2008). PROCESS OPTIMIZATION OF CL-20 PREPARATION. JOURNAL OF ENERGETIC MATERIALS, 2(2), 3-14. SID. https://sid.ir/paper/115374/en

Vancouver: Copy

BAYAT Y., ABRISHAMI F., DEHGHANI H.. PROCESS OPTIMIZATION OF CL-20 PREPARATION. JOURNAL OF ENERGETIC MATERIALS[Internet]. 2008;2(2):3-14. Available from: https://sid.ir/paper/115374/en

IEEE: Copy

Y. BAYAT, F. ABRISHAMI, and H. DEHGHANI, “PROCESS OPTIMIZATION OF CL-20 PREPARATION,” JOURNAL OF ENERGETIC MATERIALS, vol. 2, no. 2, pp. 3–14, 2008, [Online]. Available: https://sid.ir/paper/115374/en

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