1,1-SPECTROPHOTOMETRIC DETERMINATION OF TRACE AMOUNTS OF DIMETHYLHYDRAZINE (UDMH) IN MICELLAR MEDIA

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ZAREI A.R.; SABERI MOGHADDAM A.; CHALAVI S.

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Journal: JOURNAL OF ENERGETIC MATERIALS Year:2010 | Volume:4 | Issue:2 Page(s): 3-9

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Title

1,1-SPECTROPHOTOMETRIC DETERMINATION OF TRACE AMOUNTS OF DIMETHYLHYDRAZINE (UDMH) IN MICELLAR MEDIA

Author(s)

ZAREI A.R. | SABERI MOGHADDAM A. | CHALAVI S. | Issue Writer Certificate

Keywords

SPECTROPHOTOMETRIC DETERMINATIONQ3

1Q4

1-DIMETHYLHYDRAZINEQ4

MICELLAR MEDIAQ4

UDMHQ4

Abstract

1,1-DIMETHYLHYDRAZINE (unsymmetrical dimethylhydrazine, UDMH) is one of the hydrazine derivatives that is mainly used as a high-energy fuel in military applications as a rocket propellant and as a fuel for thrusters, and small electrical power generating units. 1,1-DIMETHYLHYDRAZINE is volatile and toxic, and is readily absorbed by oral, dermal or inhalation routes of exposure. Because of the environmental and toxicological significance of 1,1-DIMETHYLHYDRAZINE, sensitive and reliable analytical methods are necessary for determination of 1,1-DIMETHYLHYDRAZINE in samples. In this paper, a new spectrophotometric method for the determination of trace amounts of 1,1-DIMETHYLHYDRAZINE is described. The method is based on the reaction of 1,1-DIMETHYLHYDRAZINE with p-nitrobenzaldehyde in MICELLAR MEDIA. The optimal reaction conditions were studied and the analytical characteristics of the method were obtained. The method allowed the determination of 1,1-DIMETHYLHYDRAZINE at concentration between 0.40 - 6.0 mg.mL-1 with detection Limit (DL) of 0.1 mg.mL-1 and relative standard deviation of 1.45%, respectively. Under working conditions, the proposed method was successfully applied to the determination of 1,1-DIMETHYLHYDRAZINE in water samples.

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APA: Copy

ZAREI, A.R., SABERI MOGHADDAM, A., & CHALAVI, S.. (2010). 1,1-SPECTROPHOTOMETRIC DETERMINATION OF TRACE AMOUNTS OF DIMETHYLHYDRAZINE (UDMH) IN MICELLAR MEDIA. JOURNAL OF ENERGETIC MATERIALS, 4(2), 3-9. SID. https://sid.ir/paper/115400/en

Vancouver: Copy

ZAREI A.R., SABERI MOGHADDAM A., CHALAVI S.. 1,1-SPECTROPHOTOMETRIC DETERMINATION OF TRACE AMOUNTS OF DIMETHYLHYDRAZINE (UDMH) IN MICELLAR MEDIA. JOURNAL OF ENERGETIC MATERIALS[Internet]. 2010;4(2):3-9. Available from: https://sid.ir/paper/115400/en

IEEE: Copy

A.R. ZAREI, A. SABERI MOGHADDAM, and S. CHALAVI, “1,1-SPECTROPHOTOMETRIC DETERMINATION OF TRACE AMOUNTS OF DIMETHYLHYDRAZINE (UDMH) IN MICELLAR MEDIA,” JOURNAL OF ENERGETIC MATERIALS, vol. 4, no. 2, pp. 3–9, 2010, [Online]. Available: https://sid.ir/paper/115400/en

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