CHROMATOGRAPHIC DETERMINATION OF TRACE AMOUNTS OF HMX, RDX AND TNT COMPOUNDS IN WATER SAMPLES AFTER CLOUD POINT EXTRACTION

Q: How can I download an article?

To download an article from SID, first log in to the site, search for the article title, and click on the 'Download Article' option.

Q: How can I download an ISI article?

To download an ISI article on SID, enter the keyword or article title in the search bar, view the relevant results, click on the desired article, and select the 'Download Article' option.

Q: How can I access the SID database?

To access the SID database, visit SID.ir, create an account, and log in to access scientific resources.

Q: Is downloading articles from SID free?

Some articles on SID are available for free, while others require payment. Details are specified on the article's page.

BABAEI SAEID; ZAREEI A.R.

Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

Paper Information

Journal: JOURNAL OF ENERGETIC MATERIALS Year:2009 | Volume:3 | Issue:2 Page(s): 51-58

Download Full-Text

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Persian Verion

View:

1,461

Download:

Cites:

Information Journal Paper

Title

CHROMATOGRAPHIC DETERMINATION OF TRACE AMOUNTS OF HMX, RDX AND TNT COMPOUNDS IN WATER SAMPLES AFTER CLOUD POINT EXTRACTION

Author(s)

BABAEI SAEID | ZAREEI A.R. | Issue Writer Certificate

Keywords

SECONDARY EXPLOSIVESQ4

HMXQ4

RDXQ4

TNTQ4

CLOUD POINT EXTRACTIONQ4

HIGH PERFORMANCE LIQUID CHROMATOGRAPHYQ4

Abstract

Explosive compounds are known to release a significant plume containing toxic levels (mgL-1 to mgL-1 range) and environmental pollution of military munitions sites are hazardous to agricultural crops and humans. HMX, RDX and TNT are major ingredients in nearly every ammunition formulation and are the SECONDARY EXPLOSIVES used in greatest quantities. Since the explosives are found at ultra trace levels in environment samples, so prior to their determination an enrichment process is required and afterwards rapid and sensitive techniques for their monitoring are needed.In this work, an analytical method was developed to the preconcentration of the explosive compounds (HMX, RDX and TNT) in water samples based on the CLOUD POINT EXTRACTION, and after extraction, the extracted compounds were analysed by HIGH PERFORMANCE LIQUID CHROMATOGRAPHY. The parameters affecting extraction efficiency (such as concentrations of Triton X-1l4 and Cetyl-trimethylammonium bromide, electrolyte and its amount, temperature, incubation time, and centrifuge time) and chromatographic conditions (such as selected wavelength, nature of mobile phase and gradient program) were evaluated and optimized. Under the optimum conditions, the improvement factors of 34, 29, 61 and detection limits of 0.1, 0.14, and 0.08 mGc-1 were obtained for HMX, RDX and TNT respectively. This method was successfully applied for the determination of trace amounts of these compounds in water samples.

Cites

No record.

References

No record.

Cite

APA: Copy

BABAEI, SAEID, & ZAREEI, A.R.. (2009). CHROMATOGRAPHIC DETERMINATION OF TRACE AMOUNTS OF HMX, RDX AND TNT COMPOUNDS IN WATER SAMPLES AFTER CLOUD POINT EXTRACTION. JOURNAL OF ENERGETIC MATERIALS, 3(2), 51-58. SID. https://sid.ir/paper/115413/en

Vancouver: Copy

BABAEI SAEID, ZAREEI A.R.. CHROMATOGRAPHIC DETERMINATION OF TRACE AMOUNTS OF HMX, RDX AND TNT COMPOUNDS IN WATER SAMPLES AFTER CLOUD POINT EXTRACTION. JOURNAL OF ENERGETIC MATERIALS[Internet]. 2009;3(2):51-58. Available from: https://sid.ir/paper/115413/en

IEEE: Copy

SAEID BABAEI, and A.R. ZAREEI, “CHROMATOGRAPHIC DETERMINATION OF TRACE AMOUNTS OF HMX, RDX AND TNT COMPOUNDS IN WATER SAMPLES AFTER CLOUD POINT EXTRACTION,” JOURNAL OF ENERGETIC MATERIALS, vol. 3, no. 2, pp. 51–58, 2009, [Online]. Available: https://sid.ir/paper/115413/en

Related Journal Papers