EXPERIMENTAL KINETIC OPTIMIZATION OF CATALYTIC LIQUID PHASE HYDROGENATION OF NDMA TO UDMH

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GORJI M.

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

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Journal: JOURNAL OF ENERGETIC MATERIALS Year:2011 | Volume:6 | Issue:1 (11) Page(s): 63-71

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Title

EXPERIMENTAL KINETIC OPTIMIZATION OF CATALYTIC LIQUID PHASE HYDROGENATION OF NDMA TO UDMH

Author(s)

GORJI M. | Issue Writer Certificate

Keywords

KINETICQ2

NITROSO DIMETHYLAMINEQ3

UNSYMMETRICAL DIMETHYL HYDRAZIXNEQ3

CATALYTIC HYDROGENATIONQ3

Abstract

The hydrogenation KINETIC of NDMA to UDMH on a 5% Pd/C in aqueous solution of NDMA was studied and optimum conditions of the reaction for maximum yield of UDMH in the presence of undesired dimethyl amine (DMA) product was investigated. Experiments were carried out in a semi-batch three phase stirred tank reactor under constant pressure of 15 bar, temperature of 40 to 70°C and NDMA concentration of 40 to 70 wt%. Effects of temperature, pressure and NDMA concentration on yield of UDMH product in presence of undesired dimethylamine (DMA) were studied and the optimum conditions for selective production of UDMH were obtained. For these optimum conditions, a KINETIC scheme based upon Eley-Rideal (ER) model was proposed to predict UDMH and DMA production rates. Based on this model, the reaction parameters for these two products were estimated and the activation energies of these two reactions were determined.

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APA: Copy

GORJI, M.. (2011). EXPERIMENTAL KINETIC OPTIMIZATION OF CATALYTIC LIQUID PHASE HYDROGENATION OF NDMA TO UDMH. JOURNAL OF ENERGETIC MATERIALS, 6(1 (11)), 63-71. SID. https://sid.ir/paper/115423/en

Vancouver: Copy

GORJI M.. EXPERIMENTAL KINETIC OPTIMIZATION OF CATALYTIC LIQUID PHASE HYDROGENATION OF NDMA TO UDMH. JOURNAL OF ENERGETIC MATERIALS[Internet]. 2011;6(1 (11)):63-71. Available from: https://sid.ir/paper/115423/en

IEEE: Copy

M. GORJI, “EXPERIMENTAL KINETIC OPTIMIZATION OF CATALYTIC LIQUID PHASE HYDROGENATION OF NDMA TO UDMH,” JOURNAL OF ENERGETIC MATERIALS, vol. 6, no. 1 (11), pp. 63–71, 2011, [Online]. Available: https://sid.ir/paper/115423/en

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