OPTIMIZATION OF THE EFFECTIVE PARAMETERS ON THE SYNTHESIS OF NITRO-HTPB

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GHAYENI H.; ABUSAIDI H.; MOTAMED SHARIATI S.H.

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Journal: JOURNAL OF ENERGETIC MATERIALS Year:2015 | Volume:10 | Issue:2 (26) Page(s): 65-72

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Title

OPTIMIZATION OF THE EFFECTIVE PARAMETERS ON THE SYNTHESIS OF NITRO-HTPB

Author(s)

GHAYENI H. | ABUSAIDI H. | MOTAMED SHARIATI S.H. | Issue Writer Certificate

Keywords

NITRO FUNCTIONALIZATIONQ2

NITRO-HTPB PREPOLYMERQ2

NITRILE IODIDE REAGENTQ2

DIFFERENTIAL SCANNING CALORIMETRYQ2

Abstract

NITRO FUNCTIONALIZATION of alkenes has particular importance in the field of energetic materials due to unsaturated nature and the ability to synthesize a wide range of C-nitro aliphatic compounds. Considering the importance of these compounds, the use of nitrile iodide as a mild, inexpensive and safe reagent to NITRO FUNCTIONALIZATION of HTPB as an unsaturated prepolymer was studied in this paper. In order to optimization of the effective parameters on the synthesis of Nitro-HTPB, the proportional amounts of reactant, amount of solvent, temperature and reaction time were investigated and the effect of these parameters on the efficiency of nitro functionalized products was evaluated. It was observed that the kind and amount of solvent have a significant impact on the quality of product. In this regard, 24 hours of reaction time at room temperature were considered as optimal conditions. Finally, DIFFERENTIAL SCANNING CALORIMETRY (DSC) method was used to study the effect of the amount of nitro group on the thermal behavior of the products. It was observed that by increasing the nitro group amount of products, thermal stability decreases and heat of decomposition increases.

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APA: Copy

GHAYENI, H., ABUSAIDI, H., & MOTAMED SHARIATI, S.H.. (2015). OPTIMIZATION OF THE EFFECTIVE PARAMETERS ON THE SYNTHESIS OF NITRO-HTPB. JOURNAL OF ENERGETIC MATERIALS, 10(2 (26)), 65-72. SID. https://sid.ir/paper/115456/en

Vancouver: Copy

GHAYENI H., ABUSAIDI H., MOTAMED SHARIATI S.H.. OPTIMIZATION OF THE EFFECTIVE PARAMETERS ON THE SYNTHESIS OF NITRO-HTPB. JOURNAL OF ENERGETIC MATERIALS[Internet]. 2015;10(2 (26)):65-72. Available from: https://sid.ir/paper/115456/en

IEEE: Copy

H. GHAYENI, H. ABUSAIDI, and S.H. MOTAMED SHARIATI, “OPTIMIZATION OF THE EFFECTIVE PARAMETERS ON THE SYNTHESIS OF NITRO-HTPB,” JOURNAL OF ENERGETIC MATERIALS, vol. 10, no. 2 (26), pp. 65–72, 2015, [Online]. Available: https://sid.ir/paper/115456/en

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