INVESTIGATION ON THE EFFECT OF AL ADDITION ON SYNTHESIS OF TI3SIC2 NANOSTRUCTURE BY MECHANICAL ALLOYING- HEAT TREATMENT METHOD

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ATAZADEH N.; SAEEDI HEYDARI M.; BAHARVANDI H.R.; EHSANI N.

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Journal: JOURNAL OF NEW MATERIALS Year:2018 | Volume:8 | Issue:2 (30) Page(s): 15-28

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Title

INVESTIGATION ON THE EFFECT OF AL ADDITION ON SYNTHESIS OF TI3SIC2 NANOSTRUCTURE BY MECHANICAL ALLOYING- HEAT TREATMENT METHOD

Author(s)

ATAZADEH N. | SAEEDI HEYDARI M. | BAHARVANDI H.R. | EHSANI N. | Issue Writer Certificate

Keywords

MAX PHASEQ1

TI3SIC2Q2

MECHANICAL ALLOYING - HEAT TREATMENTQ2

MOLAR PERCENT OF ALUMINUMQ2

Abstract

In this study, the effect of Al addition in synthesis of Ti3SiC2 nanostrucure has been studied by MECHANICAL ALLOYING - HEAT TREATMENT method and using the mixture of Ti, Si, C powders. The composition of 3Ti: 1.3Si: 2C: xAl (x=0%, 0.5%, 1% and 1.5%) were used in order to evaluate the MOLAR PERCENT OF ALUMINUM in synthesis of Ti3SiC2 MAX PHASE. First the initial powders were weighed. Then, the powder mixtures were milled at the ball to powder ratio of 30: 1 for 40 hours under argon atmosphere. After that they have been formed in pills under 200 MPa pressure. After the heat treatment of the samples at 1200oC for 1 hour, an X-ray diffraction analysis was used to examine phase composition while a field emission scattering electron microscope equipped with an EDS spectrometer was utilized to observe the microstructure. The results indicate that the maximum amount of the synthesized Ti3SiC2 MAX PHASE is totally equal to 75wt.% and it is related to the sample of 3Ti: 1.3Si: 2C: xAl (x=1%) which heat treated at the temperature of 1200oC. It was also observed that the weight percentage of the Ti3SiC2 MAX PHASE has decreased in the reaction products by increasing of the MOLAR PERCENT OF ALUMINUM from 1 to 1.5 %.

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References

THE STUDY OF PARAMETERS AFFECTING THE SINTERING OF AL2O3-TIB2 NANOCOMPOSITE SYNTHESIZED VIA MECHANOCHEMICAL SYNTHESIS METHOD AND EVALUTION MECHANICAL PROPERTIES

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APA: Copy

ATAZADEH, N., SAEEDI HEYDARI, M., BAHARVANDI, H.R., & EHSANI, N.. (2018). INVESTIGATION ON THE EFFECT OF AL ADDITION ON SYNTHESIS OF TI₃SIC₂ NANOSTRUCTURE BY MECHANICAL ALLOYING- HEAT TREATMENT METHOD. JOURNAL OF NEW MATERIALS, 8(2 (30) ), 15-28. SID. https://sid.ir/paper/169704/en

Vancouver: Copy

ATAZADEH N., SAEEDI HEYDARI M., BAHARVANDI H.R., EHSANI N.. INVESTIGATION ON THE EFFECT OF AL ADDITION ON SYNTHESIS OF TI₃SIC₂ NANOSTRUCTURE BY MECHANICAL ALLOYING- HEAT TREATMENT METHOD. JOURNAL OF NEW MATERIALS[Internet]. 2018;8(2 (30) ):15-28. Available from: https://sid.ir/paper/169704/en

IEEE: Copy

N. ATAZADEH, M. SAEEDI HEYDARI, H.R. BAHARVANDI, and N. EHSANI, “INVESTIGATION ON THE EFFECT OF AL ADDITION ON SYNTHESIS OF TI₃SIC₂ NANOSTRUCTURE BY MECHANICAL ALLOYING- HEAT TREATMENT METHOD,” JOURNAL OF NEW MATERIALS, vol. 8, no. 2 (30) , pp. 15–28, 2018, [Online]. Available: https://sid.ir/paper/169704/en

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