Synthesis, and characterization of a novel derivative of dimer calix[4] arene as an artificial receptor for derivative of Alanine

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Hassibi Elham; TAGHVAEI GANJALI SAEED; Mahmoodi Hashemi Mohammad; Zadmard Reza; Moradi Dehaghi Shahram

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Journal: Journal of Applied Research in Chemistry Year:2019 | Volume:13 | Issue:2 Page(s): 99-108

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Title

Synthesis, and characterization of a novel derivative of dimer calix[4] arene as an artificial receptor for derivative of Alanine

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Keywords

Calix[4]monoquinoneQ1

Dimer calix[4]areneQ1

Artificial receptor moleculeQ1

AlanineQ1

N-Boc-AlanineQ1

Abstract

In this research, a new derivative of dimer calix[4]arene has been designed and synthesized and its molecular structure has been investigated by IR, 1HNMR, 13CNMR, Mass spectroscopy, and Elemental analyses. These studies show that this dimer calix[4]arene is a bridgeless dimer and has been synthesized from head-to-head coupling of two calix[4]monoquinone unites; two cavities of this dimer are arranged in an opposed manner and these unites to be able to host distinct for small biomolecules guests, one in each cavity as an artificial receptor, therefore a number of small biomolecules have been selected for recognition in this study and the Ultra Violet spectrophotometric technique was used to evaluate sensing ability of interaction between dimer calix[4]quinone and these guests. The results obtained from titration of visible and ultraviolet spectroscopy and association constant (KA) of calix dimer synthesized with each one of the selected guests, revealed that dimer calix[4]quinone as an artificial receptor is capable of complexing only with the N-Boc-Alanine.

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APA: Copy

Hassibi, Elham, TAGHVAEI GANJALI, SAEED, Mahmoodi Hashemi, Mohammad, Zadmard, Reza, & Moradi Dehaghi, Shahram. (2019). Synthesis, and characterization of a novel derivative of dimer calix[4] arene as an artificial receptor for derivative of Alanine. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), 13(2 ), 99-108. SID. https://sid.ir/paper/180258/en

Vancouver: Copy

Hassibi Elham, TAGHVAEI GANJALI SAEED, Mahmoodi Hashemi Mohammad, Zadmard Reza, Moradi Dehaghi Shahram. Synthesis, and characterization of a novel derivative of dimer calix[4] arene as an artificial receptor for derivative of Alanine. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC)[Internet]. 2019;13(2 ):99-108. Available from: https://sid.ir/paper/180258/en

IEEE: Copy

Elham Hassibi, SAEED TAGHVAEI GANJALI, Mohammad Mahmoodi Hashemi, Reza Zadmard, and Shahram Moradi Dehaghi, “Synthesis, and characterization of a novel derivative of dimer calix[4] arene as an artificial receptor for derivative of Alanine,” JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), vol. 13, no. 2 , pp. 99–108, 2019, [Online]. Available: https://sid.ir/paper/180258/en

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