DETERMINATION OF DIAZINON IN APPLE JUICE AND UNDERGROUND WATER USING DISPERSIVE LIQUID-LIQUID MICROEXTRACTION COUPLED WITH CORONA DISCHARGE ION MOBILITY SPECTROSCOPY

Q: How can I download an article?

To download an article from SID, first log in to the site, search for the article title, and click on the 'Download Article' option.

Q: How can I download an ISI article?

To download an ISI article on SID, enter the keyword or article title in the search bar, view the relevant results, click on the desired article, and select the 'Download Article' option.

Q: How can I access the SID database?

To access the SID database, visit SID.ir, create an account, and log in to access scientific resources.

Q: Is downloading articles from SID free?

Some articles on SID are available for free, while others require payment. Details are specified on the article's page.

JAFARI MOHAMMAD TAGHI; JAFARIAN MASOUD; SHERAFATMAND HOSSEIN

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

Paper Information

Journal: Nashrieh Shimi va Mohandesi Shimi Iran Year:2017 | Volume:36 | Issue:2 Page(s): 71-86

Download Full-Text

Persian Verion

View:

1,112

Download:

Cites:

Information Journal Paper

Title

DETERMINATION OF DIAZINON IN APPLE JUICE AND UNDERGROUND WATER USING DISPERSIVE LIQUID-LIQUID MICROEXTRACTION COUPLED WITH CORONA DISCHARGE ION MOBILITY SPECTROSCOPY

Author(s)

JAFARI MOHAMMAD TAGHI | JAFARIAN MASOUD | SHERAFATMAND HOSSEIN | Issue Writer Certificate

Keywords

DISPERSIVE LIQUID-LIQUID MICROEXTRACTIONQ1

CORONA DISCHARGE ION MOBILITY SPECTROSCOPYQ1

DIAZINONQ1

APPLEQ1

UNDERGROUND WATERQ1

Abstract

In this work, DISPERSIVE LIQUID-LIQUID MICROEXTRACTION coupled with CORONA DISCHARGE ION MOBILITY SPECTROSCOPY (DLLME-CD-IMS) was applied for the extraction and determination of DIAZINON in APPLE juice and UNDERGROUND WATER samples. For the extraction, an appropriate mixture of methanol as dispersive solvent and CCl4 as extraction solvent was injected rapidly into a glass tube with conical bottom containing an aqueous solution of DIAZINON. This injection led to a cloudy water solution, caused by the fine droplets dispersion of the immiscible extraction solvent (CCl4) in the aqueous sample. The result of this phenomenon was the generation of a high contact area between the aqueous phase and the extraction solvent. The final step of the microextraction procedure was centrifugation (5 min at 3000 rpm) to collect the dispersed tinny CCl4 droplets in the bottom of the test tube. Afterward, 5.0 mL of the solution was directly injected into the IMS, for analysis of the analyte. In order to obtain an optimum condition of the extraction, several parameters affecting on the extraction such as extraction solvent type, dispersive solvent type, extraction and dispersive solvent volume, salt addition, and pH were studied. Under optimum condition (pH 7, 60 mL extraction solvent, 1 mL dispersive solvent and without salt addition), enrichment factor 60 and the limit of detection of 0.2 mg/L was obtained. The good dynamic range was obtained in the range of 0.5-100.0 mg/L for extraction of DIAZINON. The relative standard deviations for analysis of 20 mg/L of DIAZINON in standard solutions, was 7% (n=3). The obtained recovery for spiked samples was above 89%, indicating the capability of DLLME as a rapid and convenient method for real sample analysis.

Cites

No record.

References

Cite

APA: Copy

JAFARI, MOHAMMAD TAGHI, JAFARIAN, MASOUD, & SHERAFATMAND, HOSSEIN. (2017). DETERMINATION OF DIAZINON IN APPLE JUICE AND UNDERGROUND WATER USING DISPERSIVE LIQUID-LIQUID MICROEXTRACTION COUPLED WITH CORONA DISCHARGE ION MOBILITY SPECTROSCOPY. NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN), 36(2 ), 71-86. SID. https://sid.ir/paper/26396/en

Vancouver: Copy

JAFARI MOHAMMAD TAGHI, JAFARIAN MASOUD, SHERAFATMAND HOSSEIN. DETERMINATION OF DIAZINON IN APPLE JUICE AND UNDERGROUND WATER USING DISPERSIVE LIQUID-LIQUID MICROEXTRACTION COUPLED WITH CORONA DISCHARGE ION MOBILITY SPECTROSCOPY. NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN)[Internet]. 2017;36(2 ):71-86. Available from: https://sid.ir/paper/26396/en

IEEE: Copy

MOHAMMAD TAGHI JAFARI, MASOUD JAFARIAN, and HOSSEIN SHERAFATMAND, “DETERMINATION OF DIAZINON IN APPLE JUICE AND UNDERGROUND WATER USING DISPERSIVE LIQUID-LIQUID MICROEXTRACTION COUPLED WITH CORONA DISCHARGE ION MOBILITY SPECTROSCOPY,” NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN), vol. 36, no. 2 , pp. 71–86, 2017, [Online]. Available: https://sid.ir/paper/26396/en

Related Journal Papers