Synthesis and Characterization of CexZr1-xO2 using Supercritical Water

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Golmohamadi Morteza; NASIRI HADI

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Paper Information

Journal: APPLIED RESEARCH IN CHEMICAL POLYMER ENGINEERING Year:2020 | Volume:3 | Issue:4 Page(s): 3-12

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Title

Synthesis and Characterization of CexZr1-xO2 using Supercritical Water

Author(s)

Golmohamadi Morteza | NASIRI HADI | Issue Writer Certificate

Keywords

Nanoparticle

Catalyst

Supercritical water

Mixed oxide

Characterization

Abstract

Research subject: Due to the public attention to the environmental issues as well as strict environmental regulations, eco-friendly methods for synthesis of Nanoparticles have received considerable attention in recent years. Research approach: In the present study, a Mixed oxide Nanoparticle containing cerium and zirconium (Cex-Zr1-xO2) was fabricated the in Supercritical water (SCW) medium. The synthesized Nanoparticles were characterized by various techniques, including X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Main results: Results demonstrated that fine Nanoparticles with mean size of 13± 3 nm, with high crystallinity, and with appropriate size distribution and surface area were synthesized by SCW. Moreover, an oxygen storage capacity (OSC) as high as 1. 25 mmol O2/g was estimated for Cex-Zr1-xO2 Nanoparticles through temperature programmed reduction in hydrogen (H2-TPR). According to the obtained results, the Cex-Zr1-xO2 Nanoparticles could be a suitable candidate for Catalysts of oxidation processes as well as three-way Catalyst for control of automotive exhaust gases.

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APA: Copy

Golmohamadi, Morteza, & NASIRI, HADI. (2020). Synthesis and Characterization of CexZr1-xO2 using Supercritical Water. APPLIED RESEARCH IN CHEMICAL POLYMER ENGINEERING, 3(4 ), 3-12. SID. https://sid.ir/paper/267775/en

Vancouver: Copy

Golmohamadi Morteza, NASIRI HADI. Synthesis and Characterization of CexZr1-xO2 using Supercritical Water. APPLIED RESEARCH IN CHEMICAL POLYMER ENGINEERING[Internet]. 2020;3(4 ):3-12. Available from: https://sid.ir/paper/267775/en

IEEE: Copy

Morteza Golmohamadi, and HADI NASIRI, “Synthesis and Characterization of CexZr1-xO2 using Supercritical Water,” APPLIED RESEARCH IN CHEMICAL POLYMER ENGINEERING, vol. 3, no. 4 , pp. 3–12, 2020, [Online]. Available: https://sid.ir/paper/267775/en

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