SYNTHESIS AND CHARACTERIZATION OF NANOCRYSTALLINE COAPO-5: STRUCTURAL AND MORPHOLOGICAL ANALYSIS BY ALTERATION ON HYDROTHERMAL PARAMETERS

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HASSANVAND A.; ASGHARI M.; HALAKOEI H.; RAJAEI B.

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Journal: International Journal of Nano Dimension Year:2013 | Volume:4 | Issue:1 (13) Page(s): 63-68

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Title

SYNTHESIS AND CHARACTERIZATION OF NANOCRYSTALLINE COAPO-5: STRUCTURAL AND MORPHOLOGICAL ANALYSIS BY ALTERATION ON HYDROTHERMAL PARAMETERS

Author(s)

HASSANVAND A. | ASGHARI M. | HALAKOEI H. | RAJAEI B. | Issue Writer Certificate

Keywords

NANO-ZEOLITE

COAPO-5

SYNTHESIS

CHARACTERIZATION

STRUCTURE

TEMPERATURE

Abstract

NANO-ZEOLITE COAPO-5 as a member of AFI family, was synthesized via a hydrothermal treatment, and structurally characterized using X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray analysis (EDAX). The effects of crystallization TEMPERATURE and time on the STRUCTURE of these powder products were studied. XRD patterns of the synthesized powders revealed a high-crystallinity and pure phase of AFI. SEM images and Scherrer equation showed the nano-size of the obtained COAPO-5. Also, SEM images showed nano-wires as small as 30-50 nm in COAPO-5 STRUCTUREs. According to EDAX analysis, P/Al ratio of the prepared COAPO-5 powder was about 1.5. Crystal sizes and the crystallinity of COAPO-5 reduced at higher TEMPERATUREs of hydrothermal treatment. On the other hand, the larger crystals grew by increasing the crystallization time from 24 to 48 h.

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APA: Copy

HASSANVAND, A., ASGHARI, M., HALAKOEI, H., & RAJAEI, B.. (2013). SYNTHESIS AND CHARACTERIZATION OF NANOCRYSTALLINE COAPO-5: STRUCTURAL AND MORPHOLOGICAL ANALYSIS BY ALTERATION ON HYDROTHERMAL PARAMETERS. INTERNATIONAL JOURNAL OF NANO DIMENSION (IJND), 4(1 (13)), 63-68. SID. https://sid.ir/paper/322164/en

Vancouver: Copy

HASSANVAND A., ASGHARI M., HALAKOEI H., RAJAEI B.. SYNTHESIS AND CHARACTERIZATION OF NANOCRYSTALLINE COAPO-5: STRUCTURAL AND MORPHOLOGICAL ANALYSIS BY ALTERATION ON HYDROTHERMAL PARAMETERS. INTERNATIONAL JOURNAL OF NANO DIMENSION (IJND)[Internet]. 2013;4(1 (13)):63-68. Available from: https://sid.ir/paper/322164/en

IEEE: Copy

A. HASSANVAND, M. ASGHARI, H. HALAKOEI, and B. RAJAEI, “SYNTHESIS AND CHARACTERIZATION OF NANOCRYSTALLINE COAPO-5: STRUCTURAL AND MORPHOLOGICAL ANALYSIS BY ALTERATION ON HYDROTHERMAL PARAMETERS,” INTERNATIONAL JOURNAL OF NANO DIMENSION (IJND), vol. 4, no. 1 (13), pp. 63–68, 2013, [Online]. Available: https://sid.ir/paper/322164/en

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