PRE-CONCENTRATION OF PENICILLAMINE USING FE3O4NPS AND ANALYSIS OF IT IN DRUG FORMULATIONS THROUGH SPECTROSCOPIC METHOD

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MEHRABIFAR ATEFEH; RIAHI AHMAD

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Journal: International Journal of Nano Dimension Year:2018 | Volume:9 | Issue:1 Page(s): 24-31

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Information Journal Paper

Title

PRE-CONCENTRATION OF PENICILLAMINE USING FE3O4NPS AND ANALYSIS OF IT IN DRUG FORMULATIONS THROUGH SPECTROSCOPIC METHOD

Author(s)

MEHRABIFAR ATEFEH | RIAHI AHMAD | Issue Writer Certificate

Keywords

FE3O4NPS

MAGNETIC NANOPARTICLE

PENICILLAMINE

SPECTROPHOTOMETRY

SERUM

6-DICHLOROPHENOLINDOPHENOL

Abstract

First, an effective pre-concentration of PENICILLAMINE was done via Fe3O4NPS. Then, a simple, rapid and sensitive spectrophotometric method is described for the determination of PENICILLAMINE by 2, 6-DICHLOROPHENOLINDOPHENOL (2, 6-DCPIP), as the chromogenic agent in bulk drug and formulations. It produces a bluish green coloured compound with maximum absorbance 610 nm. Beer’s law was obeyed in the concentration range 0.005-0.100 ppm with molar absorptivity 1.97 × 103 L/mol/cm and RSD 0.3-0.82%. Statistical comparison of the results with those from the reference method reveals excellent agreement and accuracy and precision was ±0.481 to ±0.33%. This method is also applied on the whole blood and SERUM samples collected from the confirmed patients. The reaction of PENICILLAMINE with 2, 6-DCPIP was confirmed by FTIR and 1H NMR. The main advantage of 2, 6-DCPIP was its stability as a reagent solution, resulting in reliable and reproducible results.

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APA: Copy

MEHRABIFAR, ATEFEH, & RIAHI, AHMAD. (2018). PRE-CONCENTRATION OF PENICILLAMINE USING FE₃O₄NPS AND ANALYSIS OF IT IN DRUG FORMULATIONS THROUGH SPECTROSCOPIC METHOD. INTERNATIONAL JOURNAL OF NANO DIMENSION (IJND), 9(1), 24-31. SID. https://sid.ir/paper/322389/en

Vancouver: Copy

MEHRABIFAR ATEFEH, RIAHI AHMAD. PRE-CONCENTRATION OF PENICILLAMINE USING FE₃O₄NPS AND ANALYSIS OF IT IN DRUG FORMULATIONS THROUGH SPECTROSCOPIC METHOD. INTERNATIONAL JOURNAL OF NANO DIMENSION (IJND)[Internet]. 2018;9(1):24-31. Available from: https://sid.ir/paper/322389/en

IEEE: Copy

ATEFEH MEHRABIFAR, and AHMAD RIAHI, “PRE-CONCENTRATION OF PENICILLAMINE USING FE₃O₄NPS AND ANALYSIS OF IT IN DRUG FORMULATIONS THROUGH SPECTROSCOPIC METHOD,” INTERNATIONAL JOURNAL OF NANO DIMENSION (IJND), vol. 9, no. 1, pp. 24–31, 2018, [Online]. Available: https://sid.ir/paper/322389/en

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