MICROWAVE-ASSISTED SOLID-PHASE (SPPS)AND SOLUTION-PHASE (SPS) SYNTHESIS OF BIOLOGICAL DIPEPTIDE ((β-ALANINE-LHISTIDINE)

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KHOSRAVI MARYAM; RAHIMI RAHMATOLLAH; RABBANI MAHBOUBEH; Safavi Ebrahim

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Journal Paper

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Journal: Journal of Applied Chemical Research Year:2017 | Volume:11 | Issue:3 Page(s): 8-18

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Information Journal Paper

Title

MICROWAVE-ASSISTED SOLID-PHASE (SPPS)AND SOLUTION-PHASE (SPS) SYNTHESIS OF BIOLOGICAL DIPEPTIDE ((β-ALANINE-LHISTIDINE)

Author(s)

KHOSRAVI MARYAM | RAHIMI RAHMATOLLAH | RABBANI MAHBOUBEH | Safavi Ebrahim | Issue Writer Certificate

Keywords

PEPTIDE

MICROWAVE

SOLUTION PHASE PEPTIDE SYNTHESIS

SOLID PHASE PEPTIDE SYNTHESIS

LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY

Abstract

PEPTIDEs have shown Promising effect as pharmaceutics with the potential to treat a wide variety of diseases. PEPTIDEs are mostly synthesized by biological technology or chemical methods. Solution phasePEPTIDE synthesis (SPS) and solid phase PEPTIDE synthesis (SPPS) are two major chemical techniques for PEPTIDEsproduction.In this research, the synthesis of dipeptde (b -alanine- L -histidine) wasexaminedby the both SPS and SPPS methods. The solution phase synthesizeswasdonebyN -phthalic anhydride as a protective group andthe solid phase using standardtert-Butyloxycarbonyl (BOC) and Fluorenylmethyloxycarbonylchloride (Fmoc).Inthe both methods, themicrowave was assisted in different steps. The molecular structure of the diPEPTIDE (b -alanine- L -histidine) wasdefined using different spectrometrymethods such as: UV-Vis, FT-IR, 1HNMR and LC-Massanalysis.

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APA: Copy

KHOSRAVI, MARYAM, RAHIMI, RAHMATOLLAH, RABBANI, MAHBOUBEH, & Safavi, Ebrahim. (2017). MICROWAVE-ASSISTED SOLID-PHASE (SPPS)AND SOLUTION-PHASE (SPS) SYNTHESIS OF BIOLOGICAL DIPEPTIDE ((β-ALANINE-LHISTIDINE). JOURNAL OF APPLIED CHEMICAL RESEARCH (JACR), 11(3), 8-18. SID. https://sid.ir/paper/323083/en

Vancouver: Copy

KHOSRAVI MARYAM, RAHIMI RAHMATOLLAH, RABBANI MAHBOUBEH, Safavi Ebrahim. MICROWAVE-ASSISTED SOLID-PHASE (SPPS)AND SOLUTION-PHASE (SPS) SYNTHESIS OF BIOLOGICAL DIPEPTIDE ((β-ALANINE-LHISTIDINE). JOURNAL OF APPLIED CHEMICAL RESEARCH (JACR)[Internet]. 2017;11(3):8-18. Available from: https://sid.ir/paper/323083/en

IEEE: Copy

MARYAM KHOSRAVI, RAHMATOLLAH RAHIMI, MAHBOUBEH RABBANI, and Ebrahim Safavi, “MICROWAVE-ASSISTED SOLID-PHASE (SPPS)AND SOLUTION-PHASE (SPS) SYNTHESIS OF BIOLOGICAL DIPEPTIDE ((β-ALANINE-LHISTIDINE),” JOURNAL OF APPLIED CHEMICAL RESEARCH (JACR), vol. 11, no. 3, pp. 8–18, 2017, [Online]. Available: https://sid.ir/paper/323083/en

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