A Developed Electromembrane Technique Based on Flat Electrospun Membrane Coupled with Gaschromatography for the Determination of Phthalates in Different Water Samples

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MOLLAHOSSEINI A.; Konh M.

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

Paper Information

Journal: Journal of Sciences, Islamic Republic of Iran Year:2019 | Volume:30 | Issue:4 Page(s): 315-323

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Title

A Developed Electromembrane Technique Based on Flat Electrospun Membrane Coupled with Gaschromatography for the Determination of Phthalates in Different Water Samples

Author(s)

MOLLAHOSSEINI A. | Konh M. | Issue Writer Certificate

Keywords

Central composite designQ1

EectrospinningQ1

Flat membraneQ1

Gas-chromatographyQ3

PhthalatesQ1

Abstract

In this work, we successfully developed electromembrane extraction via preparation of an electrospun Flat membrane based on device. The polyurethane-membrane was prepared by electrospinning method and used in EME. Affecting parameters on membrane preparation were optimized by Taguchi design. The developed method was used for extraction of Phthalates as typical molecules and the proposed method was used to determine Phthalates in water samples. The applied voltage, extraction time, distance of electrodes and agitation rate were selected as the main factors in EME and optimized using response surface methodology based on a Central composite design. Under optimum conditions, calibration curves were obtained in the range of 0. 5-5000 ng mL-1 2 with R >0. 990. The repeatabilities were less than 12% and 14% for intra-day and inter-day, respectively. The limits of detection were found to be 0. 03 and 0. 02 ng mL-1 and limits of quantification were obtained 0. 09 and 0. 06 for bis (2-ethylhexyl phthalate), and dimethyl phthalate, respectively.

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APA: Copy

MOLLAHOSSEINI, A., & Konh, M.. (2019). A Developed Electromembrane Technique Based on Flat Electrospun Membrane Coupled with Gaschromatography for the Determination of Phthalates in Different Water Samples. JOURNAL OF SCIENCES ISLAMIC REPUBLIC OF IRAN, 30(4 ), 315-323. SID. https://sid.ir/paper/369244/en

Vancouver: Copy

MOLLAHOSSEINI A., Konh M.. A Developed Electromembrane Technique Based on Flat Electrospun Membrane Coupled with Gaschromatography for the Determination of Phthalates in Different Water Samples. JOURNAL OF SCIENCES ISLAMIC REPUBLIC OF IRAN[Internet]. 2019;30(4 ):315-323. Available from: https://sid.ir/paper/369244/en

IEEE: Copy

A. MOLLAHOSSEINI, and M. Konh, “A Developed Electromembrane Technique Based on Flat Electrospun Membrane Coupled with Gaschromatography for the Determination of Phthalates in Different Water Samples,” JOURNAL OF SCIENCES ISLAMIC REPUBLIC OF IRAN, vol. 30, no. 4 , pp. 315–323, 2019, [Online]. Available: https://sid.ir/paper/369244/en

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