Synthesis of Ti3AlC2 MAX phase by MASHS

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Akhlaghi Maryam; TAYEBIFARD SEYED ALI; SALAHI ESMAEIL; Shahedi Asl Mehdi; Schmidt Gert

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Journal: METALLURGICAL ENGINEERING Year:2019 | Volume:22 | Issue:1 (73) Page(s): 65-74

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Title

Synthesis of Ti3AlC2 MAX phase by MASHS

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Keywords

Mechanical activationQ2

Self-propagating high-temperature synthesisQ1

MAX phaseQ1

Ti3AlC2Q1

Abstract

Titanium aluminum carbide was prepared employing mechanically activated Self-propagating high-temperature synthesis process. The formation mechanism of Ti3AlC2 MAX phase using elemental titanium, aluminum and carbon (graphite) powders synthesized via two different preparation methods, wave propagation and thermal explosion synthesis techniques, were investigated. The combustion reaction products were characterized by differential thermal analysis, scanning electron microscopy and X-ray diffraction analysis. Although Ti3AlC2 was recognized as the dominant synthesis product, in both techniques, the formation of TiC was also verified as a byproduct. The MAX phase produced in the tubular furnace (thermal explosion mode) was purer than that synthesized in the reaction chamber (wave propagation mode). The results disclosed that the formation of TiC and TiAl compounds have significant roles on the combustion synthesis of Ti3AlC2 MAX phase.

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APA: Copy

Akhlaghi, Maryam, TAYEBIFARD, SEYED ALI, SALAHI, ESMAEIL, Shahedi Asl, Mehdi, & Schmidt, Gert. (2019). Synthesis of Ti3AlC2 MAX phase by MASHS. METALLURGICAL ENGINEERING, 22(1 (73) ), 65-74. SID. https://sid.ir/paper/389695/en

Vancouver: Copy

Akhlaghi Maryam, TAYEBIFARD SEYED ALI, SALAHI ESMAEIL, Shahedi Asl Mehdi, Schmidt Gert. Synthesis of Ti3AlC2 MAX phase by MASHS. METALLURGICAL ENGINEERING[Internet]. 2019;22(1 (73) ):65-74. Available from: https://sid.ir/paper/389695/en

IEEE: Copy

Maryam Akhlaghi, SEYED ALI TAYEBIFARD, ESMAEIL SALAHI, Mehdi Shahedi Asl, and Gert Schmidt, “Synthesis of Ti3AlC2 MAX phase by MASHS,” METALLURGICAL ENGINEERING, vol. 22, no. 1 (73) , pp. 65–74, 2019, [Online]. Available: https://sid.ir/paper/389695/en

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