Synthesis, Characterization and Thermal Study of a High Energetic Copper(II) Complex with Triazolic Ligand

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HOSSEINI S.G.; Moeini K.

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Journal: JOURNAL OF ENERGETIC MATERIALS Year:2019 | Volume:14 | Issue:1 (41) Page(s): 55-60

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Title

Synthesis, Characterization and Thermal Study of a High Energetic Copper(II) Complex with Triazolic Ligand

Author(s)

HOSSEINI S.G. | Moeini K. | Issue Writer Certificate

Keywords

TriazoleQ1

Copper ComplexQ1

Thermal BehaviorQ2

High Energetic ComplexQ1

Spectral CharacterizationQ1

Abstract

A new high energetic copper(II) complex, [Cu(μ-DAMT)Cl2]2, was prepared by the reaction of 4, 5-diamino-3-methyl-4H-1, 2, 4-triazol-1-ium chloride (DAMT. HCl) with copper(II) nitrate and identified by elemental analysis, Spectral Characterization (FT-IR), melting point and molar conductivity. The spectral and physical characterizations of the product confirm the formation of a binuclear structure of copper(II). In the predicted structure of the complex, copper atom has a coordination number of four with a square planar geometry and CuN2Cl2 environment. In the Copper Complex, the DAMT ligand acts as N2-donor through its 2 and 3 triazolic sp2 nitrogen atoms. The amine nitrogen atoms do not participate in the coordination process. Thermal property of the ligand and complex was studied by TGA/DSC thermogram. These data reveals that although the salty ligand has an endothermic decomposition whilst after coordination to the copper atom, forms a High Energetic Complex with exothermic decomposition. This complex releases – 279. 08 Jg– 1 energy during the second step of decomposition in thermal range of 262-271 ° C.

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APA: Copy

HOSSEINI, S.G., & Moeini, K.. (2019). Synthesis, Characterization and Thermal Study of a High Energetic Copper(II) Complex with Triazolic Ligand. JOURNAL OF ENERGETIC MATERIALS, 14(1 (41) ), 55-60. SID. https://sid.ir/paper/390820/en

Vancouver: Copy

HOSSEINI S.G., Moeini K.. Synthesis, Characterization and Thermal Study of a High Energetic Copper(II) Complex with Triazolic Ligand. JOURNAL OF ENERGETIC MATERIALS[Internet]. 2019;14(1 (41) ):55-60. Available from: https://sid.ir/paper/390820/en

IEEE: Copy

S.G. HOSSEINI, and K. Moeini, “Synthesis, Characterization and Thermal Study of a High Energetic Copper(II) Complex with Triazolic Ligand,” JOURNAL OF ENERGETIC MATERIALS, vol. 14, no. 1 (41) , pp. 55–60, 2019, [Online]. Available: https://sid.ir/paper/390820/en

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