SYNTHESIS AND CRYSTAL STRUCTURE OF A NEW THIOSEMICARBZONE, ACENAPHTHENEQUINONE THIOSEMICARBAZONE MONO METHANOL

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TADJARODI A.; NAJJARI S.; NOTASH B.

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Journal: Iranian Journal of Crystallography and Mineralogy Year:2015 | Volume:22 | Issue:4 Page(s): 109-114

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Title

SYNTHESIS AND CRYSTAL STRUCTURE OF A NEW THIOSEMICARBZONE, ACENAPHTHENEQUINONE THIOSEMICARBAZONE MONO METHANOL

Author(s)

TADJARODI A. | NAJJARI S. | NOTASH B. | Issue Writer Certificate

Keywords

THIOSEMICARBAZONEQ2

C RYSTAL STRUCTUREQ2

ACENAPHTHENEQUINONEQ2

MONOCLINICQ2

Abstract

A new thiosemicarbzone compound was prepared by the reaction of ACENAPHTHENEQUINONE and thiosemicarbazide (1: 1 molar ratio) in absolute methanol at 70oC. The crystal structure of this compound, ACENAPHTHENEQUINONE THIOSEMICARBAZONE mono methanol, was determined by X-ray crystallography. The unit cell parameters are as follows: a =7.0384 (14) Å’, b =14.202 Å’, c =14.270 (3) Å’b=104.26 (3) o. It crystallizes in a MONOCLINIC system, with space group P21/c and four molecules in the unit cell. The final R value is 0.0738 for 2422 independent reflection. Both inter and intramolecular hydrogen bonds exist in crystalline system.

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APA: Copy

TADJARODI, A., NAJJARI, S., & NOTASH, B.. (2015). SYNTHESIS AND CRYSTAL STRUCTURE OF A NEW THIOSEMICARBZONE, ACENAPHTHENEQUINONE THIOSEMICARBAZONE MONO METHANOL. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, 22(4), 109-114. SID. https://sid.ir/paper/3926/en

Vancouver: Copy

TADJARODI A., NAJJARI S., NOTASH B.. SYNTHESIS AND CRYSTAL STRUCTURE OF A NEW THIOSEMICARBZONE, ACENAPHTHENEQUINONE THIOSEMICARBAZONE MONO METHANOL. IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY[Internet]. 2015;22(4):109-114. Available from: https://sid.ir/paper/3926/en

IEEE: Copy

A. TADJARODI, S. NAJJARI, and B. NOTASH, “SYNTHESIS AND CRYSTAL STRUCTURE OF A NEW THIOSEMICARBZONE, ACENAPHTHENEQUINONE THIOSEMICARBAZONE MONO METHANOL,” IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, vol. 22, no. 4, pp. 109–114, 2015, [Online]. Available: https://sid.ir/paper/3926/en

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