SYNTHESIS AND CRYSTAL STRUCTURE OF SCHIFF-BASE COMPOUNDS N-(3, 4-DIMETHOXYBENZYLIDENE)-4-METHOXYANILINE (1) AND N-(3, 4-DIMETHOXYBENZYLIDENE)-4-ETHOXYANILINE (2)

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DEHNO KHALAJI ALIAKBAR; FEJFAROVA KARLA; DUSEK MICHAL

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Journal: Iranian Journal of Crystallography and Mineralogy Year:2011 | Volume:19 | Issue:2 Page(s): 41-46

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Title

SYNTHESIS AND CRYSTAL STRUCTURE OF SCHIFF-BASE COMPOUNDS N-(3, 4-DIMETHOXYBENZYLIDENE)-4-METHOXYANILINE (1) AND N-(3, 4-DIMETHOXYBENZYLIDENE)-4-ETHOXYANILINE (2)

Author(s)

DEHNO KHALAJI ALIAKBAR | FEJFAROVA KARLA | DUSEK MICHAL | Issue Writer Certificate

Keywords

SCHIFF-BASEQ2

CRYSTAL STRUCTUREQ2

MONOCLINICQ2

Abstract

New SCHIFF-BASE compounds N-(3, 4-dimethoxybenzylidene)-4-methoxyaniline (1) and N-(3, 4-dimethoxybenzylidene)-4-ethoxyaniline (2) were synthesized and characterized by elemental analyses (CHN) and FT-IR spectroscopic techniques. CRYSTAL STRUCTUREs of 1 and 2 were obtained by single-crystal Xray diffraction. Compound 1 crystallizes in the MONOCLINIC, space group P21 with two independent molecules (A and B), with unit cell parameters: a=14.8198 (4), b=7.1656 (2), c=13.2982 (4) A, b=103.289 (2)o, V=1374.36 (7) A3 and Z=4 and compound 2 crystallizes in the MONOCLINIC space group P21/n with unit cell parameters: a=16.5638 (6), b=7.3546 (2), c=12.7449 (4) A, b=106.021 (4)o, V=1492.28 (9) A3 and Z=4.

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APA: Copy

DEHNO KHALAJI, ALIAKBAR, FEJFAROVA, KARLA, & DUSEK, MICHAL. (2011). SYNTHESIS AND CRYSTAL STRUCTURE OF SCHIFF-BASE COMPOUNDS N-(3, 4-DIMETHOXYBENZYLIDENE)-4-METHOXYANILINE (1) AND N-(3, 4-DIMETHOXYBENZYLIDENE)-4-ETHOXYANILINE (2). IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, 19(2), 41-46. SID. https://sid.ir/paper/394027/en

Vancouver: Copy

DEHNO KHALAJI ALIAKBAR, FEJFAROVA KARLA, DUSEK MICHAL. SYNTHESIS AND CRYSTAL STRUCTURE OF SCHIFF-BASE COMPOUNDS N-(3, 4-DIMETHOXYBENZYLIDENE)-4-METHOXYANILINE (1) AND N-(3, 4-DIMETHOXYBENZYLIDENE)-4-ETHOXYANILINE (2). IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY[Internet]. 2011;19(2):41-46. Available from: https://sid.ir/paper/394027/en

IEEE: Copy

ALIAKBAR DEHNO KHALAJI, KARLA FEJFAROVA, and MICHAL DUSEK, “SYNTHESIS AND CRYSTAL STRUCTURE OF SCHIFF-BASE COMPOUNDS N-(3, 4-DIMETHOXYBENZYLIDENE)-4-METHOXYANILINE (1) AND N-(3, 4-DIMETHOXYBENZYLIDENE)-4-ETHOXYANILINE (2),” IRANIAN JOURNAL OF CRYSTALLOGRAPHY AND MINERALOGY, vol. 19, no. 2, pp. 41–46, 2011, [Online]. Available: https://sid.ir/paper/394027/en

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