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Information Journal Paper

Title

Design and Synthesis of New 19-25 Membered Aza-Macrocycles Based on 2, 4, 6-Triarylpyridine

Pages

  87-95

Abstract

 Formation of macrocycle from non-cyclic precursors is inherently difficult. In this research, to minimizing of this problem, two methods, crab-like, and Template-directed synthesis were run together simultaneously, to afford new eleven aza macrocycles (AM1-11) based on 2, 4, 6-Triaryl pyridine in high yields. The AM1-11 were synthesized by the reaction of diamine compounds (1-11) with 2, 6-bis(3-(2-chloroacetamido)phenyl)-4-(phenyl)pyridine (BCP) as a crab-like reagent, in the presence of K2CO3/KI (Template reagent). BCP was obtained from the reaction of 2, 6-Bis(3-aminophenyl)-4-(phenyl)pyridine (BAP) and chloro acetylchloride at room temperature. Also, BAP was synthesized by using 3-nitro acetophenone and bezaldehyde in the manner of modified Chichibabin reaction and then the reduction of the product by Zn/NH4Cl. The structures of macrocycles were confirmed by IR, 1H NMR, 13C NMR, and Mass spectroscopies.

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    • Cite

    APA: Copy

    KAMALI, MAHMOOD. (2021). Design and Synthesis of New 19-25 Membered Aza-Macrocycles Based on 2, 4, 6-Triarylpyridine. NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN), 39(4 (98) ), 87-95. SID. https://sid.ir/paper/411089/en

    Vancouver: Copy

    KAMALI MAHMOOD. Design and Synthesis of New 19-25 Membered Aza-Macrocycles Based on 2, 4, 6-Triarylpyridine. NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN)[Internet]. 2021;39(4 (98) ):87-95. Available from: https://sid.ir/paper/411089/en

    IEEE: Copy

    MAHMOOD KAMALI, “Design and Synthesis of New 19-25 Membered Aza-Macrocycles Based on 2, 4, 6-Triarylpyridine,” NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN), vol. 39, no. 4 (98) , pp. 87–95, 2021, [Online]. Available: https://sid.ir/paper/411089/en

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