Investigation of calcination temperature on the structural, optical and photocatalytic properties of mesoporous titania nanoparticles

Q: How can I download an article?

To download an article from SID, first log in to the site, search for the article title, and click on the 'Download Article' option.

Q: How can I download an ISI article?

To download an ISI article on SID, enter the keyword or article title in the search bar, view the relevant results, click on the desired article, and select the 'Download Article' option.

Q: How can I access the SID database?

To access the SID database, visit SID.ir, create an account, and log in to access scientific resources.

Q: Is downloading articles from SID free?

Some articles on SID are available for free, while others require payment. Details are specified on the article's page.

Gorgani Mahtab; KOOZEGAR KALEJI BEHZAD

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

Paper Information

Journal: Journal of Applied Research in Chemistry Year:2020 | Volume:14 | Issue:1 Page(s): 69-79

Download Full-Text

Persian Verion

View:

225

Download:

Cites:

Information Journal Paper

Title

Investigation of calcination temperature on the structural, optical and photocatalytic properties of mesoporous titania nanoparticles

Author(s)

Gorgani Mahtab | KOOZEGAR KALEJI BEHZAD | Issue Writer Certificate

Keywords

Titanium dioxideQ2

Calcination temperatureQ1

MesoporousQ1

Photocatalytic degradationQ1

Optical propertiesQ2

Abstract

In this study, Mesoporous Titanium dioxide nanoparticles were synthesized by sol-gel method. The effect of Calcination temperature on structural, photocatalytic, and Optical properties of nanoparticles was investigated. Tetrabutylorthotitanate )TBT( was used as a precursor of titanium and ethanol as a solvent. Differential thermal analysis )TG-DTA( for selecting the appropriate temperature range for calcination, phase analysis by X-ray diffraction )XRD(, BET analysis for the specific surface area and porosity of the nanoparticles, spectrophotometric analysis for the study of photocatalytic properties, and scanning electron microscopy structural characteristics including morphology and particle size were used. The results show that by increasing the temperature up to 550 ° C, anatase phase transformation into rutile is performed, and the presence of two crystalline phases improves photocatalytic properties. The band gap energy of Titanium dioxide nanoparticles has decreased with increasing temperature, so that shifted from the ultraviolet range to the visible light range. The highest degradation percentage of ultraviolet radiation was obtained by sample with Calcination temperature of 350 ° C )57. 33%( and was exposed to visible light with a Calcination temperature of 550 ° C )55. 56%(. The results of adsorption analysis indicated the Mesoporous structure with H4 and H2 type hysteresis loop for the samples prepared at 350 ° C and 550 ° C, respectively. The average pore diameters for the samples prepared at 350 ° C and 550 ° C were 1. 20 and 7. 99 nm, respectively. The TEM images indicated that the particle size of the samples prepared at 350 ° C and 550 ° C were 25-30 nm and 30-45 nm, respectively.

Cites

No record.

References

No record.

Cite

APA: Copy

Gorgani, Mahtab, & KOOZEGAR KALEJI, BEHZAD. (2020). Investigation of calcination temperature on the structural, optical and photocatalytic properties of mesoporous titania nanoparticles. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), 14(1 ), 69-79. SID. https://sid.ir/paper/411739/en

Vancouver: Copy

Gorgani Mahtab, KOOZEGAR KALEJI BEHZAD. Investigation of calcination temperature on the structural, optical and photocatalytic properties of mesoporous titania nanoparticles. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC)[Internet]. 2020;14(1 ):69-79. Available from: https://sid.ir/paper/411739/en

IEEE: Copy

Mahtab Gorgani, and BEHZAD KOOZEGAR KALEJI, “Investigation of calcination temperature on the structural, optical and photocatalytic properties of mesoporous titania nanoparticles,” JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), vol. 14, no. 1 , pp. 69–79, 2020, [Online]. Available: https://sid.ir/paper/411739/en

Related Journal Papers

No record.

Related Seminar Papers

No record.

Related Plans

No record.

Recommended Workshops