APPLICATION OF POLYPYRROLE COATED STAINLESS-STEEL WIRE TO THE HEADSPACE SOLID-PHASE MICROEXTRACTION OF ALIPHATIC AMINES

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KEYKHAEI M.R.; SAFARI F.

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

Paper Information

Journal: Journal of Sciences, Islamic Republic of Iran Year:2008 | Volume:19 | Issue:2 Page(s): 111-117

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Information Journal Paper

Title

APPLICATION OF POLYPYRROLE COATED STAINLESS-STEEL WIRE TO THE HEADSPACE SOLID-PHASE MICROEXTRACTION OF ALIPHATIC AMINES

Author(s)

KEYKHAEI M.R. | SAFARI F. | Issue Writer Certificate

Keywords

CAPILLARY GAS CHROMATOGRAPHY

HEADSPACE SOLID PHASE MICROEXTRACTION

VOLATILE ALIPHATIC AMINES

POLYPYRROLE COATING

Abstract

The electrochemical coating technique was used for the preparation of a POLYPYRROLE COATING on a stainless-steel wire, and applied as a fibre for solid phase microextraction (SPME). The polypyrrole fibre was employed for analyzing four VOLATILE ALIPHATIC AMINES (ethylamine, propylamine, butylamine and pentylamine) in water by headspace SPME using gas chromatography-flame ionization detection (GC-FID). Results showed that this fibre coating is suitable for the successful extraction of the target analytes. The effects of the extraction parameters including exposure time, sampling temperature, salt concentration, and stirring rate on the extraction efficiency was optimized. Relative standard deviations (RSDs) were determined ≤4.3%. The correlation coefficient was satisfactory (r2 > 0.98) for the studied analytes. Detection limits were between 0.9 and 1.6mg.L-1. Good recoveries (99-106 %) were obtained when spiked water and wastewater samples were analyzed

Cites

ORDERED NANOPOROUS CARBON BASED SOLID-PHASE MICROEXTRACTION FOR THE ANALYSIS OF NITROAROMATIC COMPOUNDS IN AQUEOUS SAMPLES

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APA: Copy

KEYKHAEI, M.R., & SAFARI, F.. (2008). APPLICATION OF POLYPYRROLE COATED STAINLESS-STEEL WIRE TO THE HEADSPACE SOLID-PHASE MICROEXTRACTION OF ALIPHATIC AMINES. JOURNAL OF SCIENCES ISLAMIC REPUBLIC OF IRAN, 19(2), 111-117. SID. https://sid.ir/paper/561037/en

Vancouver: Copy

KEYKHAEI M.R., SAFARI F.. APPLICATION OF POLYPYRROLE COATED STAINLESS-STEEL WIRE TO THE HEADSPACE SOLID-PHASE MICROEXTRACTION OF ALIPHATIC AMINES. JOURNAL OF SCIENCES ISLAMIC REPUBLIC OF IRAN[Internet]. 2008;19(2):111-117. Available from: https://sid.ir/paper/561037/en

IEEE: Copy

M.R. KEYKHAEI, and F. SAFARI, “APPLICATION OF POLYPYRROLE COATED STAINLESS-STEEL WIRE TO THE HEADSPACE SOLID-PHASE MICROEXTRACTION OF ALIPHATIC AMINES,” JOURNAL OF SCIENCES ISLAMIC REPUBLIC OF IRAN, vol. 19, no. 2, pp. 111–117, 2008, [Online]. Available: https://sid.ir/paper/561037/en

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