PREPARATION AND CHARACTERIZATION OF HYPERBRANCHED POLYSTYRENE NANOCOMPOSITE SYNTHESIZED BY LIVING RADICAL POLYMERIZATION AND SOLUTION INTERCALATION METHOD

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ABBASIAN MOJTABA; FATHI ASGHAR; ENTEZAMI ALI AKBAR; JAYMAND MEHDI

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Paper Information

Journal: Iranian Journal of Polymer Science and Technology Year:2012 | Volume:24 | Issue:6 (ISSUE NUMBER 116) Page(s): 434-443

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Title

PREPARATION AND CHARACTERIZATION OF HYPERBRANCHED POLYSTYRENE NANOCOMPOSITE SYNTHESIZED BY LIVING RADICAL POLYMERIZATION AND SOLUTION INTERCALATION METHOD

Author(s)

ABBASIAN MOJTABA | FATHI ASGHAR | ENTEZAMI ALI AKBAR | JAYMAND MEHDI | Issue Writer Certificate

Keywords

POLYSTYRENEQ2

POLYMETHYL METHACRYLATEQ3

ATRPQ2

LAPONITE RDQ2

NANOCOMPOSITEQ2

Abstract

AcoPolymer of styrene and methyl styrene was synthesized by nitroxide-mediated "living" free radical polymerization (NMP). N-Bromosuccinimide was used as a brominating agent to obtain a copolymer with bromine as its end group. This brominated copolymer was used as macro initiators for atom transfer radical polymerization (ATRP). Chemical modification of the clay and transformation of this inorganic material to an organophilic clay was carried out by cation exchange reaction between the clay and hexadecyl trimethyl ammonium chloride salt in deionized water by mechanical stirring. Preparation of NANOCOMPOSITE was carried out by solution intercalation method. The structures of the terpolymer and other compounds were investigated by IHNMR, GPC, FTIR, SEM, TEM and XRD methods and their thermal stability was examined by TGA analyses.

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APA: Copy

ABBASIAN, MOJTABA, FATHI, ASGHAR, ENTEZAMI, ALI AKBAR, & JAYMAND, MEHDI. (2012). PREPARATION AND CHARACTERIZATION OF HYPERBRANCHED POLYSTYRENE NANOCOMPOSITE SYNTHESIZED BY LIVING RADICAL POLYMERIZATION AND SOLUTION INTERCALATION METHOD. IRANIAN JOURNAL OF POLYMER SCIENCE AND TECHNOLOGY (PERSIAN), 24(6 (ISSUE NUMBER 116)), 434-443. SID. https://sid.ir/paper/6353/en

Vancouver: Copy

ABBASIAN MOJTABA, FATHI ASGHAR, ENTEZAMI ALI AKBAR, JAYMAND MEHDI. PREPARATION AND CHARACTERIZATION OF HYPERBRANCHED POLYSTYRENE NANOCOMPOSITE SYNTHESIZED BY LIVING RADICAL POLYMERIZATION AND SOLUTION INTERCALATION METHOD. IRANIAN JOURNAL OF POLYMER SCIENCE AND TECHNOLOGY (PERSIAN)[Internet]. 2012;24(6 (ISSUE NUMBER 116)):434-443. Available from: https://sid.ir/paper/6353/en

IEEE: Copy

MOJTABA ABBASIAN, ASGHAR FATHI, ALI AKBAR ENTEZAMI, and MEHDI JAYMAND, “PREPARATION AND CHARACTERIZATION OF HYPERBRANCHED POLYSTYRENE NANOCOMPOSITE SYNTHESIZED BY LIVING RADICAL POLYMERIZATION AND SOLUTION INTERCALATION METHOD,” IRANIAN JOURNAL OF POLYMER SCIENCE AND TECHNOLOGY (PERSIAN), vol. 24, no. 6 (ISSUE NUMBER 116), pp. 434–443, 2012, [Online]. Available: https://sid.ir/paper/6353/en

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