APPLICATION OF RESPONSE SURFACE METHODOLOGY FOR CATALYTIC HYDROGENATION OF NITROBENZENE TO ANILINE USING RUTHENIUM SUPPORTED FULLERENE NANOCATALYST

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KEYPOUR HASSAN; NOROOZI MOHAMMAD; RASHIDI ALIMORAD; SHARIATI RAD MASOUD

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Journal: Iranian Journal of Chemistry and Chemical Engineering Year:2015 | Volume:34 | Issue:1 Page(s): 21-32

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Title

APPLICATION OF RESPONSE SURFACE METHODOLOGY FOR CATALYTIC HYDROGENATION OF NITROBENZENE TO ANILINE USING RUTHENIUM SUPPORTED FULLERENE NANOCATALYST

Author(s)

KEYPOUR HASSAN | NOROOZI MOHAMMAD | RASHIDI ALIMORAD | SHARIATI RAD MASOUD | Issue Writer Certificate

Keywords

HYDROGENATION

NITROBENZENE

ANILINE

RUTHENIUM

FULLERENE

RESPONSE SURFACE METHODOLOGY

Abstract

In this study FULLERENE functionalized using oleum (H2SO4·SO3), followed by the hydrolysis of the intermediate cyclosulfated FULLERENE as well as an oxidizing agent was employed to functionalize the FULLERENEs. RUTHENIUM was then added by the impregnation method or deposited on the functionalized FULLERENE. Subsequent to this step, RESPONSE SURFACE METHODOLOGY (RSM) was used to study the cumulative effect of various parameters including, pressure, temperature, time and loading. In order to maximize the HYDROGENATION of NITROBENZENE (NB) to ANILINE (AN) these latter parameters were optimized. Furthermore, catalytic activity was evaluated over a temperature range of 25–150oC, hydrogen pressure of 1-30 atm, RUTHENIUM content of 1-15% (w/w) and reaction time of 30-180 min in a bench scale reactor. The optimized model predicted that the HYDROGENATION should be at a maximum level (approximately 100%) with the following conditions; Ru loading of 15%, reaction temperature of 150oC, reaction time of 180 min and hydrogen pressure of 22.33 atm.

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APA: Copy

KEYPOUR, HASSAN, NOROOZI, MOHAMMAD, RASHIDI, ALIMORAD, & SHARIATI RAD, MASOUD. (2015). APPLICATION OF RESPONSE SURFACE METHODOLOGY FOR CATALYTIC HYDROGENATION OF NITROBENZENE TO ANILINE USING RUTHENIUM SUPPORTED FULLERENE NANOCATALYST. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 34(1), 21-32. SID. https://sid.ir/paper/635669/en

Vancouver: Copy

KEYPOUR HASSAN, NOROOZI MOHAMMAD, RASHIDI ALIMORAD, SHARIATI RAD MASOUD. APPLICATION OF RESPONSE SURFACE METHODOLOGY FOR CATALYTIC HYDROGENATION OF NITROBENZENE TO ANILINE USING RUTHENIUM SUPPORTED FULLERENE NANOCATALYST. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2015;34(1):21-32. Available from: https://sid.ir/paper/635669/en

IEEE: Copy

HASSAN KEYPOUR, MOHAMMAD NOROOZI, ALIMORAD RASHIDI, and MASOUD SHARIATI RAD, “APPLICATION OF RESPONSE SURFACE METHODOLOGY FOR CATALYTIC HYDROGENATION OF NITROBENZENE TO ANILINE USING RUTHENIUM SUPPORTED FULLERENE NANOCATALYST,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 34, no. 1, pp. 21–32, 2015, [Online]. Available: https://sid.ir/paper/635669/en

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