SYNTHESIS AND STRUCTURE DETERMINATION OF NOVEL DERIVATIVE OF CYCLOTRIPHOSPHAZENE WITH PHLOROGLUSINE LIGAND WITH TWO PROTECTED POSITION

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PAPAN AZADEH; TARASSOLI ABBAS; SHAHIDIAN ZAHRA

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Journal Paper

Paper Information

Journal: Iranian Journal of Chemistry and Chemical Engineering Year:2016 | Volume:35 | Issue:2 Page(s): 1-7

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Information Journal Paper

Title

SYNTHESIS AND STRUCTURE DETERMINATION OF NOVEL DERIVATIVE OF CYCLOTRIPHOSPHAZENE WITH PHLOROGLUSINE LIGAND WITH TWO PROTECTED POSITION

Author(s)

PAPAN AZADEH | TARASSOLI ABBAS | SHAHIDIAN ZAHRA | Issue Writer Certificate

Keywords

HEXACHLOROTRIPHOSPHAZENE

PHLOROGLUSINE

OXYGEN-CONTAINING LIGAND

TOSYL CHLORIDE

PHOSPHAZENE

Abstract

In this study we have been involved in the synthesis and characterization studies of a new cyclotriorganophosphazenes complex with protected PHLOROGLUSINE ligand. Firstly, we synthesized hexachlorocyclotirphosphazene from ammonium chloride and phosphorus pentachloride reaction and then two hydroxyl groups of the PHLOROGLUSINE ligand were protected with methyl iodide and TOSYL CHLORIDE. Finally, the deprotonated and protected PHLOROGLUSINE was reacted as an OXYGEN-CONTAINING LIGAND with hexachlorocyclotriphosphazene in the ratio of 6: 1 in THF as a solvent, All of Cl atoms were substituted with hydroxyl groups of ligand to give a new product. This product identified by a series of spectroscopic techniques including FT-IR, 31P NMR, 13C NMR, 1H NMR and mass spectrometry.

Cites

SYNTHESIS OF A NOVEL CYCLOTRIPHOSPHAZENE BY USING XANTHYDROL OXYGEN CONTAINING LIGAND

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APA: Copy

PAPAN, AZADEH, TARASSOLI, ABBAS, & SHAHIDIAN, ZAHRA. (2016). SYNTHESIS AND STRUCTURE DETERMINATION OF NOVEL DERIVATIVE OF CYCLOTRIPHOSPHAZENE WITH PHLOROGLUSINE LIGAND WITH TWO PROTECTED POSITION. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), 35(2), 1-7. SID. https://sid.ir/paper/686069/en

Vancouver: Copy

PAPAN AZADEH, TARASSOLI ABBAS, SHAHIDIAN ZAHRA. SYNTHESIS AND STRUCTURE DETERMINATION OF NOVEL DERIVATIVE OF CYCLOTRIPHOSPHAZENE WITH PHLOROGLUSINE LIGAND WITH TWO PROTECTED POSITION. IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE)[Internet]. 2016;35(2):1-7. Available from: https://sid.ir/paper/686069/en

IEEE: Copy

AZADEH PAPAN, ABBAS TARASSOLI, and ZAHRA SHAHIDIAN, “SYNTHESIS AND STRUCTURE DETERMINATION OF NOVEL DERIVATIVE OF CYCLOTRIPHOSPHAZENE WITH PHLOROGLUSINE LIGAND WITH TWO PROTECTED POSITION,” IRANIAN JOURNAL OF CHEMISTRY AND CHEMICAL ENGINEERING (IJCCE), vol. 35, no. 2, pp. 1–7, 2016, [Online]. Available: https://sid.ir/paper/686069/en

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