FACILE AND RAPID SYNTHESIS OF SOME OPTICALLY ACTIVE IMIDE-ACID DERIVATIVES USING MICROWAVE IRRADIATION

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FAGHIHI KH.

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Journal: JOURNAL OF SCIENCES (ISLAMIC AZAD UNIVERSITY) Year:2007 | Volume:17 | Issue:64 (CHEMISTRY ISUE) Page(s): 2-6

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Title

FACILE AND RAPID SYNTHESIS OF SOME OPTICALLY ACTIVE IMIDE-ACID DERIVATIVES USING MICROWAVE IRRADIATION

Author(s)

FAGHIHI KH. | Issue Writer Certificate

Keywords

MICROWAVE-ASSISTED REACTIONQ3

OPTICALLY ACTIVE IMIDE-ACIDSQ3

(ALPHA)-AMINO ACIDSQ3

Abstract

Imide acid derivatives are an important class of substrates for biological and chemical applications. In the chemical applications they are used for synthesis of new amino acid derivatives and peptides. In this paper rapid and highly efficient synthesis of six optically active imide-acid derivatives 4(a-f) was achieved under microwave irradiation by using a domestic microwave oven from the reactions of six different chiral a-amino acid 2(a-f) with phthalic anhydide 1 in the presence of small amount of N,N-dimethyl formamide (DMF) as a base. The reaction proceeded rapidly (100-150 sec), and as a result a series of chiral imideacid derivatives 4(a-f) were obtained in high yields (96-100%). All of the synthesized compounds were fully characterized by their melting point, specific rotations, elemental analyses, 1H-NMR and FT-IR spectroscopy.

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APA: Copy

FAGHIHI, KH.. (2007). FACILE AND RAPID SYNTHESIS OF SOME OPTICALLY ACTIVE IMIDE-ACID DERIVATIVES USING MICROWAVE IRRADIATION. JOURNAL OF SCIENCES (ISLAMIC AZAD UNIVERSITY), 17(64 (CHEMISTRY ISUE)), 2-6. SID. https://sid.ir/paper/70374/en

Vancouver: Copy

FAGHIHI KH.. FACILE AND RAPID SYNTHESIS OF SOME OPTICALLY ACTIVE IMIDE-ACID DERIVATIVES USING MICROWAVE IRRADIATION. JOURNAL OF SCIENCES (ISLAMIC AZAD UNIVERSITY)[Internet]. 2007;17(64 (CHEMISTRY ISUE)):2-6. Available from: https://sid.ir/paper/70374/en

IEEE: Copy

KH. FAGHIHI, “FACILE AND RAPID SYNTHESIS OF SOME OPTICALLY ACTIVE IMIDE-ACID DERIVATIVES USING MICROWAVE IRRADIATION,” JOURNAL OF SCIENCES (ISLAMIC AZAD UNIVERSITY), vol. 17, no. 64 (CHEMISTRY ISUE), pp. 2–6, 2007, [Online]. Available: https://sid.ir/paper/70374/en

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