SYNTHESISE AND CHARACTRIZATION OF CRISTALINE STRUCTURE OF VANADIUM COMPLEXE WITH 2-PYRIDINE CARBOXALDEHYDE SCHIFF BASE

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Naziri Mir A.; SAHIN E.; SHAABANI B.

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Seminar Paper

Paper Information

Seminar: SYMPOSIUM OF CRYSTALLOGRAPHY AND MINERALOGY OF IRAN
Year:2016 | Issue:23

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Title

SYNTHESISE AND CHARACTRIZATION OF CRISTALINE STRUCTURE OF VANADIUM COMPLEXE WITH 2-PYRIDINE CARBOXALDEHYDE SCHIFF BASE

Author(s)

Naziri Mir A. | SAHIN E. | SHAABANI B.

Keywords

CRYSTALLOGRAPHY

SCHIFF BASE

VANADIUM

HYDRAZIDE

PYRIDINE

Abstract

X-RAY CRYSTALLOGRAPHIC STUDIES LED TO THE DISCOVERY OF EVEN MORE EXOTIC TYPES OF BONDING IN INORGANIC CHEMISTRY, SUCH AZ METAL-METAL DOUBLE BONDS, METAL-METAL QUADRUPLE BONDS, AND THREE-CENTER, TWO-ELECTRON BONDS.THE CHEMISTRY OF VANADIUM (V) IS DOMINATED BY THE STABLE OXOVANADIUM CATION (VO+3) WHICH REMAINS INTACT DURING MANY REACTIONS. THE REDOX PROPERTIES OF VO (SALEN) IN ACETONITRYLE IN THE PRESENCE OF PERCHLORIC ACID AND PROVIDED EVIDENCE OF WHAT THEY TOOK TO BE THE DISPORTIONATION OF VO (SALEN) TO VO (SALEN)+. OXOVANADIUM (IV) DERIVATIVES HAVE BEEN USED AS CATALYSTS IN THE EPOXIDATION OF OLEFINS AND IN THE OXIDATION OF SULFIDES WITH PEROXIDES. IN THIS RESERCH THE LIGAND 4-HYDROXYBENZHYDRAZIDE AND 2- PYRIDINE CARBOXALDEHYDE (L) HAS BEEN PREPARED BY CONDENSATION OF 4-HYDROXYBENZHYDRAZIDE WITH 2- PYRIDINE CARBOXALDEHYDE RESPECTIVELY IN THE ABSOLUT ETHANOL AS SOLVENT. VO-COMPLEXE, VOL OF THISE LIGAND WERE SYNTHESIZED BY REACTIONS OF NH4VO3 WITH LIGAND. THE LIGAND AND ITS COMPLEXE WERE CHARACTERIZED BY X-RAY, FT-IR, UV-VIS, 1H-NMR, ANALYSE. AND AT LEAST CHEMICAL BEHEVIOR OF LIGAND AND ITS COMPLEX WERE HAVE BEEN INVESTIGATED.

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APA: Copy

Naziri, Mir A., SAHIN, E., & SHAABANI, B.. (2016). SYNTHESISE AND CHARACTRIZATION OF CRISTALINE STRUCTURE OF VANADIUM COMPLEXE WITH 2-PYRIDINE CARBOXALDEHYDE SCHIFF BASE. SYMPOSIUM OF CRYSTALLOGRAPHY AND MINERALOGY OF IRAN. SID. https://sid.ir/paper/926421/en

Vancouver: Copy

Naziri Mir A., SAHIN E., SHAABANI B.. SYNTHESISE AND CHARACTRIZATION OF CRISTALINE STRUCTURE OF VANADIUM COMPLEXE WITH 2-PYRIDINE CARBOXALDEHYDE SCHIFF BASE. 2016. Available from: https://sid.ir/paper/926421/en

IEEE: Copy

Mir A. Naziri, E. SAHIN, and B. SHAABANI, “SYNTHESISE AND CHARACTRIZATION OF CRISTALINE STRUCTURE OF VANADIUM COMPLEXE WITH 2-PYRIDINE CARBOXALDEHYDE SCHIFF BASE,” presented at the SYMPOSIUM OF CRYSTALLOGRAPHY AND MINERALOGY OF IRAN. 2016, [Online]. Available: https://sid.ir/paper/926421/en

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