RECENTLY, IT WAS FOUND THAT A GROUP OF ORGANIC MOLECULES HAVING SIMILAR STRUCTURES CAN BE SEPARATED FROM EACH OTHER ACCORDING TO THEIR ADSORPTION STRENGTHS ONTO THE SURFACES OF METAL OXIDES. IRON OXIDES AND IRON HYDROXIDES HAVE ABILITY TO ADSORB GLUCOSE IN AQUEOUS SOLUTION. IT SEEMS THAT GLUCOSE BINDS WITH MINERAL SURFACES CREATES HYDROGEN BONDING.ELECTROCATALYTIC OXIDATION OF GLUCOSE HAS A CRUCIAL ROLE IN MEASURING BLOOD SUGAR BY BLOOD GLUCOSE SENSORS. METAL ELECTRODES (CU, CO, CD, AU, AG, ETC.) CAN BE USED AS AN ELECTROCATALYST FOR OXIDATION OF GLUCOSE. AG ELECTRODES HAVE A HIGH SENSITIVITY IN GLUCOSE OXIDATION. THEREFORE, IT WAS SUGGESTED THAT THE MODIFIED AG ELECTRODES WITH METAL OXIDES MIGHT BE MORE SENSITIVE TO GLUCOSE THAN THE AG ELECTRODES.. IN THIS STUDY, IRON OXIDES (FE3O4, FE2O3) AND IRON HYDROXIDES (FEOOH) NANOPARTICLES, WERE FIRSTLY SYNTHESIZED AND THEN USED AS A SUBSTRATE FOR DEPOSITION OF SILVER NANOPARTICLES. THE SYNTHESIZED HETERODIMERIC NANOPARTICLES (FE3O4-AG, FE2O3-AG AND FEOOH-AG) WERE USED AS A MODIFIER MATERIAL IN PREPARATION OF THE MODIFIED CARBON PASTE ELECTRODES. THE PREPARED ELECTRODES SHOWED HIGH AFFINITY TOWARDS GLUCOSE. THE HETRODIMERIC NANOPARTICLES WERE PHYSICALLY CHARACTERIZED BY UV-VIS SPECTROPHOTOMETRY, SCANNING ELECTRON MICROSCOPY (SEM), TRANSMISSION ELECTRON MICROSCOPY (TEM) AND X-RAY DIFFRACTION (XRD) ANALYSIS. ELECTROCHEMICAL BEHAVIORS OF THE HETERODIMERIC NANOPARTICLES WERE INVESTIGATED BY CYCLIC VOLTAMMETRY. THE NONENZYMATIC OXIDATION PEAK OF GLUCOSE AND ITS INTERMEDIATES ON THE SURFACE OF ELECTRODES (VERSUS AG/AGCL) WERE OBSERVED IN ALKALINE SOLUTION. THE RESULTS SHOWED THAT THE SENSIVITY OF THE ELECTRODE BASED ON FE3O4-AG NANOPARTICLES WAS GREATER THAN THAT OF THE ELECTRODES BASED ON THE OTHER SYNTHESIZED HETERODIMERIC NANOPARTICLES. THE EFFECTS OF VARIOUS PARAMETERS SUCH AS CARBON PASTE COMPOSITION, TYPE OF ELECTROLYTE, PH AND SCAN RATE, ON THE RESPONSE OF THE PREPARED BIOSENSOR WERE STUDIED. UNDER THE OPTIMUM CONDITIONS, THE BIOSENSOR WAS APPLIED TO DETERMINE GLUCOSE IN HUMAN SERUM.