Friction stir processing is a solid state process to modify microstructure and mechanical properties of sheet metals and as-cast materials. In this process stirring action of the tool causes the material to intense plastic deformation that yields a dynamical recrystallization. In this study the effect of FSP and process parameters on hardness, and microstructure of Al5083 has been investigated. Also by using of FSP, composite layer of TiO2/Al5083 has been produced. Results show that, FSP leads to finer and homogenized grain structure, as well as increased hardness, strength, toughness, and elongation of material. The composites produced by FSP have uniformly distribution of TiO2 particles between the grains of base metal.