SYNTHESIS, IDENTIFICATION AND CONFORMATIONAL ANALYSIS OF NEW DERIVATIVES OF HYDROXYETHYL TETRAZOLES AS ENERGETIC DIOLS

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SHAHIDZADEH M.; FARZANDI F.

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Journal: JOURNAL OF ENERGETIC MATERIALS Year:2014 | Volume:9 | Issue:2 (23) Page(s): 27-34

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Title

SYNTHESIS, IDENTIFICATION AND CONFORMATIONAL ANALYSIS OF NEW DERIVATIVES OF HYDROXYETHYL TETRAZOLES AS ENERGETIC DIOLS

Author(s)

SHAHIDZADEH M. | FARZANDI F. | Issue Writer Certificate

Keywords

TETRAZOLEQ3

ALKYLATIONQ2

ENERGETIC MATERIALSQ2

DIOLQ2

Abstract

TETRAZOLEs and their derivatives are insensitive energetic molecules that can be used in the compounding of the high energy material. Herein, two types of bishyroxyethylTETRAZOLE compounds have been synthesized using bisnitrile and sodium azide and via consequent ALKYLATION of the reaction product. The structure of all products have been confirmed by 1HNMR, MASS spectroscopy and elemental analysis. Also, for better interpretation of the 1HNMR spectra of bishydroxy ethyl TETRAZOLE, the most stable conformation of 2-(5-methyl-2H-tetrazol-2-yl) ethan-1-ol (as a model molecule) have been investigated. The results of conformational analysis have indicated that the most stable conformation is gauch one. So, under basis of the 1HNMR and conformational analysis, the presence of an intramolecular hydrogen bond between -OH group and the 2-N atom of TETRAZOLE ring in hydroxyl ethyl TETRAZOLE compounds was confirmed.

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APA: Copy

SHAHIDZADEH, M., & FARZANDI, F.. (2014). SYNTHESIS, IDENTIFICATION AND CONFORMATIONAL ANALYSIS OF NEW DERIVATIVES OF HYDROXYETHYL TETRAZOLES AS ENERGETIC DIOLS. JOURNAL OF ENERGETIC MATERIALS, 9(2 (23)), 27-34. SID. https://sid.ir/paper/115298/en

Vancouver: Copy

SHAHIDZADEH M., FARZANDI F.. SYNTHESIS, IDENTIFICATION AND CONFORMATIONAL ANALYSIS OF NEW DERIVATIVES OF HYDROXYETHYL TETRAZOLES AS ENERGETIC DIOLS. JOURNAL OF ENERGETIC MATERIALS[Internet]. 2014;9(2 (23)):27-34. Available from: https://sid.ir/paper/115298/en

IEEE: Copy

M. SHAHIDZADEH, and F. FARZANDI, “SYNTHESIS, IDENTIFICATION AND CONFORMATIONAL ANALYSIS OF NEW DERIVATIVES OF HYDROXYETHYL TETRAZOLES AS ENERGETIC DIOLS,” JOURNAL OF ENERGETIC MATERIALS, vol. 9, no. 2 (23), pp. 27–34, 2014, [Online]. Available: https://sid.ir/paper/115298/en

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