EXPERIMENTAL AND THEORETICAL INVESTIGATION OF HEALABLE HTPB BASED POLYURETHANES BY FURAN/MALEIMIDE DIELS-ALDER REACTION

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SHAHIDZADEH M.; YARMOHAMADI M.; PIRHADI V.

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Journal: JOURNAL OF ENERGETIC MATERIALS Year:2016 | Volume:11 | Issue:1 (29) Page(s): 27-37

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Title

EXPERIMENTAL AND THEORETICAL INVESTIGATION OF HEALABLE HTPB BASED POLYURETHANES BY FURAN/MALEIMIDE DIELS-ALDER REACTION

Author(s)

SHAHIDZADEH M. | YARMOHAMADI M. | PIRHADI V. | Issue Writer Certificate

Keywords

HTPBQ2

BISMALEIMIDEQ2

HEALING ABILITYQ2

DIELS-ALDER REACTIONQ2

POLYURETHANEQ2

Abstract

The reversibility of the DIELS-ALDER REACTION can be used advantageously in POLYURETHANE materials to endow them with recyclable, thermally reversible properties and self-healing ability to expand their application range. In this paper, linear and crosslink POLYURETHANEs based on HTPB, which exhibit thermal reversibility through Diels-Alder and retro DIELS-ALDER REACTIONs, were prepared and characterized from the reaction of BISMALEIMIDE and furan terminated polybutadiene. Also tetrafuran cross linker is synthesized and characterized by FT- IR and 1HNMR for the preparation of Diels-Alder network.the semiempirical calculations analysis are performed to study the reversibility of the model reaction.Also, reversibility of DIELS-ALDER REACTION in the prepared POLYURETHANE was investigated through heating and cooling cycle by using differential scanning calorimetry (DSC). The results have shown that the retro DIELS-ALDER REACTION is occurred at 70 to 150oC.Evaluation of healability of prepared POLYURETHANE was done by cutting the polymer and recovering of its initial shape after reheating at 60oC.

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APA: Copy

SHAHIDZADEH, M., YARMOHAMADI, M., & PIRHADI, V.. (2016). EXPERIMENTAL AND THEORETICAL INVESTIGATION OF HEALABLE HTPB BASED POLYURETHANES BY FURAN/MALEIMIDE DIELS-ALDER REACTION. JOURNAL OF ENERGETIC MATERIALS, 11(1 (29)), 27-37. SID. https://sid.ir/paper/115324/en

Vancouver: Copy

SHAHIDZADEH M., YARMOHAMADI M., PIRHADI V.. EXPERIMENTAL AND THEORETICAL INVESTIGATION OF HEALABLE HTPB BASED POLYURETHANES BY FURAN/MALEIMIDE DIELS-ALDER REACTION. JOURNAL OF ENERGETIC MATERIALS[Internet]. 2016;11(1 (29)):27-37. Available from: https://sid.ir/paper/115324/en

IEEE: Copy

M. SHAHIDZADEH, M. YARMOHAMADI, and V. PIRHADI, “EXPERIMENTAL AND THEORETICAL INVESTIGATION OF HEALABLE HTPB BASED POLYURETHANES BY FURAN/MALEIMIDE DIELS-ALDER REACTION,” JOURNAL OF ENERGETIC MATERIALS, vol. 11, no. 1 (29), pp. 27–37, 2016, [Online]. Available: https://sid.ir/paper/115324/en

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