Effect of Chelating Agent on Morphology and Phase Evolution of Spinel Nanoparticles Synthesized via Sol-Gel Method

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Loghman Estarki m.r.; Ghalibaf Tousi H.; Mohammad Sharifi E.; Sheikh H.; Alhaji A.

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Journal: ADVANCED MATERIALS IN ENGINEERING (ESTEGHLAL) Year:2020 | Volume:38 | Issue:4 Page(s): 33-42

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Title

Effect of Chelating Agent on Morphology and Phase Evolution of Spinel Nanoparticles Synthesized via Sol-Gel Method

Author(s)

Keywords

SpinelQ2

GlycerolQ1

EthylenediamineQ1

Chelate agentQ1

Complex agentQ1

Abstract

The purpose of this study was to evaluate the effect of glycyrol (tri-dentate, GLY) and Ethylenediamine (double-dentate clay, en) chelating agents on phase and morphology changes of Spinel nanoparticles synthesized by sol-gel method. Characterization of samples was performed by X-ray diffraction (XRD) and field-emission scanning electron microscope (FESEM) equipped with energy dispersive X-ray spectrometer (EDX). The results showed that both samples synthesized with GLY and en contain cubic Spinel phase. The sample synthesized with Ethylenediamine has a pyramidal morphology with particle size in the range of 20-25 nm whereas the specimen prepared with Glycerol is spherical with particle size in the range of 20-25 nm. Finally, suggested mechanism for morphological changes of spniel nanoparticles was discussed.

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APA: Copy

Loghman Estarki, m.r., Ghalibaf Tousi, H., Mohammad Sharifi, E., Sheikh, H., & Alhaji, A.. (2020). Effect of Chelating Agent on Morphology and Phase Evolution of Spinel Nanoparticles Synthesized via Sol-Gel Method. ADVANCED MATERIALS IN ENGINEERING (ESTEGHLAL), 38(4 ), 33-42. SID. https://sid.ir/paper/163169/en

Vancouver: Copy

Loghman Estarki m.r., Ghalibaf Tousi H., Mohammad Sharifi E., Sheikh H., Alhaji A.. Effect of Chelating Agent on Morphology and Phase Evolution of Spinel Nanoparticles Synthesized via Sol-Gel Method. ADVANCED MATERIALS IN ENGINEERING (ESTEGHLAL)[Internet]. 2020;38(4 ):33-42. Available from: https://sid.ir/paper/163169/en

IEEE: Copy

m.r. Loghman Estarki, H. Ghalibaf Tousi, E. Mohammad Sharifi, H. Sheikh, and A. Alhaji, “Effect of Chelating Agent on Morphology and Phase Evolution of Spinel Nanoparticles Synthesized via Sol-Gel Method,” ADVANCED MATERIALS IN ENGINEERING (ESTEGHLAL), vol. 38, no. 4 , pp. 33–42, 2020, [Online]. Available: https://sid.ir/paper/163169/en

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