One-Pot Synthesis of Hydrophobic Silica Nano Particles with Long-Chain Alcohol 1-Octadecanol

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Dargahi Zaboli M.; SAHRAEI E.; POURABBAS B.; Korgel B.

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Journal Paper

Paper Information

Journal: Journal of Metallurgical and Materials Engineering Year:2018 | Volume:29 | Issue:1 Page(s): 11-20

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Title

One-Pot Synthesis of Hydrophobic Silica Nano Particles with Long-Chain Alcohol 1-Octadecanol

Author(s)

Dargahi Zaboli M. | SAHRAEI E. | POURABBAS B. | Korgel B. | Issue Writer Certificate

Keywords

One-Pot SynthesisQ2

Surface ModificationQ2

Silica NanoparticlesQ1

HydrophobicQ2

1-OctadecanolQ2

Stober MethodQ2

Abstract

In this work, One-Pot Synthesis of modified Silica Nanoparticles with long-chain alcohol 1-Octadecanol byStober Method at 70  C is presented. Hydrophobicity of particles increased dramatically by increasing the amount of 1-Octadecanol up to 7 wt. %. Surface Modification was completed during the first 90 minutes. Additionalreaction time had no further effect. The most possible modification was obtained when the reaction took place at pH=8. Successful Surface Modification was confirmed by FT-IR spectroscopy, thermogravimetric analyses and contact angle measurements. X-ray diffraction patterns indicate an amorphous structure which did not significantly change by Surface Modification. Transmission electron microscopy images were used to investigate the morphology and dimension of the silica particles.

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APA: Copy

Dargahi Zaboli, M., SAHRAEI, E., POURABBAS, B., & Korgel, B.. (2018). One-Pot Synthesis of Hydrophobic Silica Nano Particles with Long-Chain Alcohol 1-Octadecanol. JOURNAL OF METALLURGICAL AND MATERIALS ENGINEERING (JOURNAL OF SCHOOL OF ENGINEERING), 29(1 ), 11-20. SID. https://sid.ir/paper/196046/en

Vancouver: Copy

Dargahi Zaboli M., SAHRAEI E., POURABBAS B., Korgel B.. One-Pot Synthesis of Hydrophobic Silica Nano Particles with Long-Chain Alcohol 1-Octadecanol. JOURNAL OF METALLURGICAL AND MATERIALS ENGINEERING (JOURNAL OF SCHOOL OF ENGINEERING)[Internet]. 2018;29(1 ):11-20. Available from: https://sid.ir/paper/196046/en

IEEE: Copy

M. Dargahi Zaboli, E. SAHRAEI, B. POURABBAS, and B. Korgel, “One-Pot Synthesis of Hydrophobic Silica Nano Particles with Long-Chain Alcohol 1-Octadecanol,” JOURNAL OF METALLURGICAL AND MATERIALS ENGINEERING (JOURNAL OF SCHOOL OF ENGINEERING), vol. 29, no. 1 , pp. 11–20, 2018, [Online]. Available: https://sid.ir/paper/196046/en

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