STUDYING THE EFFECT OF N-HEXANE ON THE FORMATION OF P123 MICELLES IN THE MESOSTRUCTURED SOL OF TITANIA BY DLS TECHNIQUE

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AFZAL ALGHOM ALIEH; SAMEEI LEILA; BEITOLLAHI ALI; MIRKAZEMI SAYED MOHAMAD

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Journal: CERAMIC SCIENCE & ENGINEERING Year:2012 | Volume:1 | Issue:1 Page(s): 31-44

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Title

STUDYING THE EFFECT OF N-HEXANE ON THE FORMATION OF P123 MICELLES IN THE MESOSTRUCTURED SOL OF TITANIA BY DLS TECHNIQUE

Author(s)

AFZAL ALGHOM ALIEH | SAMEEI LEILA | BEITOLLAHI ALI | MIRKAZEMI SAYED MOHAMAD | Issue Writer Certificate

Keywords

TITANIA SOLQ3

UNIMERQ3

MICELLEQ3

MESOPOROUSQ3

SWELLING AGENTQ3

DLS TECHNIQUEQ3

Abstract

In this research, stable mesostructured TITANIA SOLs were synthesized employing P123 block copolymer as soft template under controlled hydrolysis of titanium is opropoxide (TTIP) in alcoholic media. In order to study the effect of Hexane additive on the sol characteristics and aggregation of the P 123 UNIMERs, two molar ratios of Hexane to P 123(H/P) of 60 and 240 were used in the sol composition. The effect of addition stage of Hexane to the sol and aging time (at 50oC for 1 and 14 days) on the size distribution of UNIMERic clusters were also investigated by dynamic light scattering (DLS) technique. It was shown that the stage of addition has a marked effect on the size distribution of the clusters formed. Comparison of DLS plots for the prepared sols with and without Hexane revealed a shift towards smaller sizes for the former. Further, no signs of MICELLE formation could be detected for the sample containing the highest Hexane content, based on DLS results. However, for the sample with HIP molar ratio of 60 aged for 1 and 14 days, rising sizes of the clusters close to P 123 MICELLE size was noticed. This reached to 19 nm for the sample with 60 H/Pmolar ratio aged for 14 days. Finally, MICELLE formation and micellar aggregation will be discussed for the system studied here.

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APA: Copy

AFZAL ALGHOM, ALIEH, SAMEEI, LEILA, BEITOLLAHI, ALI, & MIRKAZEMI, SAYED MOHAMAD. (2012). STUDYING THE EFFECT OF N-HEXANE ON THE FORMATION OF P123 MICELLES IN THE MESOSTRUCTURED SOL OF TITANIA BY DLS TECHNIQUE. CERAMIC SCIENCE & ENGINEERING, 1(1), 31-44. SID. https://sid.ir/paper/227888/en

Vancouver: Copy

AFZAL ALGHOM ALIEH, SAMEEI LEILA, BEITOLLAHI ALI, MIRKAZEMI SAYED MOHAMAD. STUDYING THE EFFECT OF N-HEXANE ON THE FORMATION OF P123 MICELLES IN THE MESOSTRUCTURED SOL OF TITANIA BY DLS TECHNIQUE. CERAMIC SCIENCE & ENGINEERING[Internet]. 2012;1(1):31-44. Available from: https://sid.ir/paper/227888/en

IEEE: Copy

ALIEH AFZAL ALGHOM, LEILA SAMEEI, ALI BEITOLLAHI, and SAYED MOHAMAD MIRKAZEMI, “STUDYING THE EFFECT OF N-HEXANE ON THE FORMATION OF P123 MICELLES IN THE MESOSTRUCTURED SOL OF TITANIA BY DLS TECHNIQUE,” CERAMIC SCIENCE & ENGINEERING, vol. 1, no. 1, pp. 31–44, 2012, [Online]. Available: https://sid.ir/paper/227888/en

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