The effect of nano transition metals on microstructure and phase evolution of low carbon MgO-C refractories

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RASTEGAR HOSSEIN; BAVAND VANDCHALI MOHAMMAD; NEMATI ALI; GOLESTANI FARD FARHAD

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Journal: CERAMIC SCIENCE & ENGINEERING Year:2019 | Volume:8 | Issue:3 Page(s): 19-28

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Title

The effect of nano transition metals on microstructure and phase evolution of low carbon MgO-C refractories

Author(s)

RASTEGAR HOSSEIN | BAVAND VANDCHALI MOHAMMAD | NEMATI ALI | GOLESTANI FARD FARHAD | Issue Writer Certificate

Keywords

Fe nano particlesQ1

CatalystQ2

CNTsQ1

Ceramic whiskersQ1

Abstract

In the present study, the effect of Iron Nitrate as catalytic precursor to in situ formation of nano-Fe particles in phenolic resin and microstructural evolution of MgO-C refractories has been investigated. Therefore, various samples according to matrix section formulation of low carbon MgO-C refractories (LCMCR’ s) with 0 and 6 wt% (Fe/Phenolic resin) were prepared and phase and microstructure changes after coking at temperatures 800-1400º C studied by XRD and FESEM analyses. Based on attained results, iron nitrate transfer to Fe nano particles with 60-80 nm in diameter during firing in reduced atmosphere. In situ formed Fe nano-particles as catalytic agent promotes graphitization behavior of phenolic resins. Increasing temperature led to a more effective graphitization level. In addition, the different nano crystalline carbon shapes such as onion and bamboo like and carbon nanotubes (CNTs) were in situ formed. Phase and microstructure analysis of LCMCR’ s samples reveal that different Ceramic whiskers such as MgO, MgAl2O4 spinel, Al4C3 and AlN formed after coking at 1000 º C and the amount of whiskers phases significantly increased at higher coking temperatures. It was also clarified the presence of Fe nano-particles have effective influence on the formation of gases components and promote ceramic phases formation. Microstructural observation showed the graphitic carbons like carbon nano-tubes (CNTs) and Ceramic whiskers mainly formed in the bonding phase between the aggregates according to the V-L-S and V-S growth mechanism.

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APA: Copy

RASTEGAR, HOSSEIN, BAVAND VANDCHALI, MOHAMMAD, NEMATI, ALI, & GOLESTANI FARD, FARHAD. (2019). The effect of nano transition metals on microstructure and phase evolution of low carbon MgO-C refractories. CERAMIC SCIENCE & ENGINEERING, 8(3 ), 19-28. SID. https://sid.ir/paper/227907/en

Vancouver: Copy

RASTEGAR HOSSEIN, BAVAND VANDCHALI MOHAMMAD, NEMATI ALI, GOLESTANI FARD FARHAD. The effect of nano transition metals on microstructure and phase evolution of low carbon MgO-C refractories. CERAMIC SCIENCE & ENGINEERING[Internet]. 2019;8(3 ):19-28. Available from: https://sid.ir/paper/227907/en

IEEE: Copy

HOSSEIN RASTEGAR, MOHAMMAD BAVAND VANDCHALI, ALI NEMATI, and FARHAD GOLESTANI FARD, “The effect of nano transition metals on microstructure and phase evolution of low carbon MgO-C refractories,” CERAMIC SCIENCE & ENGINEERING, vol. 8, no. 3 , pp. 19–28, 2019, [Online]. Available: https://sid.ir/paper/227907/en

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