Substitution of Zinc Cation in Nickel Ferrite Synthesized by Sol-Gel Method and Evaluation of its Effect on Microwave Absorption, Structural and Magnetic Properties

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Tahmasebi Shirin; EBRAHIMI KAHRIZSANGI REZA; GHASEMI ALI; GHASEMI EBRAHIM

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Journal: Journal of Advanced Processes in Materials Engineering Year:2020 | Volume:14 | Issue:3 (54) Page(s): 41-50

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Title

Substitution of Zinc Cation in Nickel Ferrite Synthesized by Sol-Gel Method and Evaluation of its Effect on Microwave Absorption, Structural and Magnetic Properties

Author(s)

Tahmasebi Shirin | EBRAHIMI KAHRIZSANGI REZA | GHASEMI ALI | GHASEMI EBRAHIM | Issue Writer Certificate

Keywords

Nickel FerriteQ2

Zinc FerriteQ1

MagnetizationQ1

Coercive ForceQ1

Abstract

In this study, the effect of substitution of Ni with Zn cation on the structural and magnetic characteristics of Nickel Ferrite prepared by sol-gel method was investigated. X-ray diffraction analysis (XRD), field emission scanning electron microscopy (FESEM), energy dispersive spectroscopy (EDS), Fourier transform infrared spectroscopy (FTIR), vibrating sample magnetometer (VSM) and vector network analyzer were used to investigate the structural, magnetic and microwave properties of ferrite particles. For Nickel Ferrite doped with zinc cation, Single-phase temperature was detected 1200 oC. Single-phase doped ferrite was obtained without any impurities and secondary phase. FESEM images showed an increase in particle size with increasing Zn cation substitution. EDS Results showed an increase in the Zn peak and a decrease in the Ni peak intensity with increasing in Zn substitution. FTIR peaks in confirmation with XRD results showed the formation of the spinel phase and the replacement of metal cations in the spinel structure. Magnetic hysteresis curves showed an increase in saturation of Magnetization and remanent Magnetization up to x = 0. 6 and then a decrease to x = 1. The magnetic Coercive Force has always a decreasing trend up to x = 0. 8 and then an increase in x = 1. Reflection loss versus frequency diagrams for doped samples showed an increase in microwave absorption.

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APA: Copy

Tahmasebi, Shirin, EBRAHIMI KAHRIZSANGI, REZA, GHASEMI, ALI, & GHASEMI, EBRAHIM. (2020). Substitution of Zinc Cation in Nickel Ferrite Synthesized by Sol-Gel Method and Evaluation of its Effect on Microwave Absorption, Structural and Magnetic Properties. ADVANCED PROCESSES IN MATERIALS, 14(3 (54) ), 41-50. SID. https://sid.ir/paper/364288/en

Vancouver: Copy

Tahmasebi Shirin, EBRAHIMI KAHRIZSANGI REZA, GHASEMI ALI, GHASEMI EBRAHIM. Substitution of Zinc Cation in Nickel Ferrite Synthesized by Sol-Gel Method and Evaluation of its Effect on Microwave Absorption, Structural and Magnetic Properties. ADVANCED PROCESSES IN MATERIALS[Internet]. 2020;14(3 (54) ):41-50. Available from: https://sid.ir/paper/364288/en

IEEE: Copy

Shirin Tahmasebi, REZA EBRAHIMI KAHRIZSANGI, ALI GHASEMI, and EBRAHIM GHASEMI, “Substitution of Zinc Cation in Nickel Ferrite Synthesized by Sol-Gel Method and Evaluation of its Effect on Microwave Absorption, Structural and Magnetic Properties,” ADVANCED PROCESSES IN MATERIALS, vol. 14, no. 3 (54) , pp. 41–50, 2020, [Online]. Available: https://sid.ir/paper/364288/en

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