STEP-GROWTH POLYMERIZATION REACTION OF 4-(4-ACETAMIDOPHENYL)-1,2,4-TRIAZOLIDINE-3,5-DIONE WITH ALIPHATIC DIACID CHLORIDES

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MALAKPOUR SH.; RAFIEI ZAHRA

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

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Journal: Iranian Polymer Journal Year:2005 | Volume:14 | Issue:12 (66) Page(s): 1066-1073

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Information Journal Paper

Title

STEP-GROWTH POLYMERIZATION REACTION OF 4-(4-ACETAMIDOPHENYL)-1,2,4-TRIAZOLIDINE-3,5-DIONE WITH ALIPHATIC DIACID CHLORIDES

Author(s)

MALAKPOUR SH. | RAFIEI ZAHRA | Issue Writer Certificate

Keywords

POLYAMIDES

STEP-GROWTH POLYMERIZATION

INHERENT VISCOSITY

4-(4-ACETAMIDOPHENYL)-1

4-TRIAZOLIDINE- 3

5-DIONE

THERMOGRAVIMETRIC ANALYSIS

Abstract

4-(4-aminophenyl)-1,2,4-triazolidine-3,5-DIONE (1) was reacted with one mole of acetyl chloride in dry N,N-dimethylacetamide (DMAc) at low temperature and 4-(4-acetamidophenyl)-1,2,4-triazolidine-3,5-DIONE [4-(4-acetanilido)-1,2,4-triazolidine-3,5-DIONE] APTD (3) was obtained in high yield. The compound APTD was reacted with excess acetyl chloride in DMAc solution and gave 1,2-bis-acetyl-4-(4-acetamidophenyl)-1,2,4-triazolidine-3,5-DIONE (4) as a model compound. Solution polycondensation reactions of monomer 3 with succinyl chloride (SucC), suberoyl chloride (SubC) and sebacoyl chloride (SebC) were performed under conventional solution polymerization techniques in the presence of different catalysts and lead to the formation of novel aliphatic POLYAMIDES. These novel POLYAMIDES have inherent viscosities in a range of 0.08-0.24 dLg-1 in N,N-dimethylformamide (DMF) at 25oC. Some structural characterization and physical properties of these novel polymers are reported.

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APA: Copy

MALAKPOUR, SH., & RAFIEI, ZAHRA. (2005). STEP-GROWTH POLYMERIZATION REACTION OF 4-(4-ACETAMIDOPHENYL)-1,2,4-TRIAZOLIDINE-3,5-DIONE WITH ALIPHATIC DIACID CHLORIDES. IRANIAN POLYMER JOURNAL (ENGLISH), 14(12 (66)), 1066-1073. SID. https://sid.ir/paper/530755/en

Vancouver: Copy

MALAKPOUR SH., RAFIEI ZAHRA. STEP-GROWTH POLYMERIZATION REACTION OF 4-(4-ACETAMIDOPHENYL)-1,2,4-TRIAZOLIDINE-3,5-DIONE WITH ALIPHATIC DIACID CHLORIDES. IRANIAN POLYMER JOURNAL (ENGLISH)[Internet]. 2005;14(12 (66)):1066-1073. Available from: https://sid.ir/paper/530755/en

IEEE: Copy

SH. MALAKPOUR, and ZAHRA RAFIEI, “STEP-GROWTH POLYMERIZATION REACTION OF 4-(4-ACETAMIDOPHENYL)-1,2,4-TRIAZOLIDINE-3,5-DIONE WITH ALIPHATIC DIACID CHLORIDES,” IRANIAN POLYMER JOURNAL (ENGLISH), vol. 14, no. 12 (66), pp. 1066–1073, 2005, [Online]. Available: https://sid.ir/paper/530755/en

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