Supported Ionic Liquid on Silica Gel: A Novel Heterogeneous Catalyst for the Synthesis of α, , β,-Unsaturated Compounds

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Honarmand Moones

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Journal Paper

Paper Information

Journal: Nashrieh Shimi va Mohandesi Shimi Iran Year:2021 | Volume:40 | Issue:3 (101) Page(s): 83-88

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Information Journal Paper

Title

Supported Ionic Liquid on Silica Gel: A Novel Heterogeneous Catalyst for the Synthesis of α, , β,-Unsaturated Compounds

Author(s)

Honarmand Moones | Issue Writer Certificate

Keywords

Ionic liquid

Heterogeneous catalyst

Silica gel

Recyclable

Abstract

In this study, supported tris(hydroxymethyl)methane ammonium acetate Ionic liquid on Silica gel (SiO2-THMAA) was synthesized for the first time. SiO2-THMAA was prepared by the reaction of 3-chloropropylsilica with tris(hydroxymethyl) aminomethane followed by ion exchange with acetate. SiO2-THMAA was characterized by FT-IR, BET, and elemental analysis. Also, to explore the catalytic activity of SiO2-THMAA in organic reactions, the synthesis of α, , β,-unsaturated compounds was investigated in the presence of SiO2-THMAA as a Heterogeneous catalyst at room temperature. The desired products were produced in high yields and short times in mild reaction conditions. SiO2-THMAA was also recovered and reused after the three reaction cycle without a significant decrease in catalytic activity.

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APA: Copy

Honarmand, Moones. (2021). Supported Ionic Liquid on Silica Gel: A Novel Heterogeneous Catalyst for the Synthesis of α, , β,-Unsaturated Compounds. NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN), 40(3 (101) ), 83-88. SID. https://sid.ir/paper/1004712/en

Vancouver: Copy

Honarmand Moones. Supported Ionic Liquid on Silica Gel: A Novel Heterogeneous Catalyst for the Synthesis of α, , β,-Unsaturated Compounds. NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN)[Internet]. 2021;40(3 (101) ):83-88. Available from: https://sid.ir/paper/1004712/en

IEEE: Copy

Moones Honarmand, “Supported Ionic Liquid on Silica Gel: A Novel Heterogeneous Catalyst for the Synthesis of α, , β,-Unsaturated Compounds,” NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN), vol. 40, no. 3 (101) , pp. 83–88, 2021, [Online]. Available: https://sid.ir/paper/1004712/en

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