Nano-cellulose-OSnCl4-x: Green and natural-based renewable nanocatalyst for one-pot synthesis of 2-amino-3-phenylsulfonyl-4H-pyran derivatives

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SHAFE MEHRABADI SAYED RASUL; SADEGHI BAHAREH; Mosslemin Mohammad Hossein; Hashemian Saeedeh

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Journal Paper

Paper Information

Journal: IRANIAN JOURNAL OF CATALYSIS Year:2022 | Volume:12 | Issue:4 Page(s): 407-416

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Information Journal Paper

Title

Nano-cellulose-OSnCl4-x: Green and natural-based renewable nanocatalyst for one-pot synthesis of 2-amino-3-phenylsulfonyl-4H-pyran derivatives

Author(s)

SHAFE MEHRABADI SAYED RASUL | SADEGHI BAHAREH | Mosslemin Mohammad Hossein | Hashemian Saeedeh | Issue Writer Certificate

Keywords

Phenylsulfonylacetonitrile

pyran derivatives

dimedone

green chemistry

nano-cellulose-OSnCl4-x

Abstract

A highly efficient, eco-friendly procedure has been proposed for the synthesis of 2-amino-3-phenylsulfonyl-4H-pyran derivatives via nano-cellulose-OSnCl4-x catalyst prepared from cotton as support treated with tin tetrachloride (SnCl4). This catalyst is characterized by FT-IR, FESEM, TEM, TGA, and EDX. The TEM results confirmed the size of the nano-cellulose-OSnCl4-x catalyst was below 30 nm. The efficiency of this solid acid catalyst was investigated in one-pot, three-component condensation reactions with aromatic aldehydes, dimedone, and Phenylsulfonylacetonitrile under reflux conditions. As a result, 2-amino-3-phenylsulfonyl-4H-pyran derivatives were produced under facile conditions in high yield (84-95%) and high rate (30-50 min) using nano-cellulose-OSnCl4-x as a recyclable catalyst.

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APA: Copy

SHAFE MEHRABADI, SAYED RASUL, SADEGHI, BAHAREH, Mosslemin, Mohammad Hossein, & Hashemian, Saeedeh. (2022). Nano-cellulose-OSnCl4-x: Green and natural-based renewable nanocatalyst for one-pot synthesis of 2-amino-3-phenylsulfonyl-4H-pyran derivatives. IRANIAN JOURNAL OF CATALYSIS, 12(4), 407-416. SID. https://sid.ir/paper/1065507/en

Vancouver: Copy

SHAFE MEHRABADI SAYED RASUL, SADEGHI BAHAREH, Mosslemin Mohammad Hossein, Hashemian Saeedeh. Nano-cellulose-OSnCl4-x: Green and natural-based renewable nanocatalyst for one-pot synthesis of 2-amino-3-phenylsulfonyl-4H-pyran derivatives. IRANIAN JOURNAL OF CATALYSIS[Internet]. 2022;12(4):407-416. Available from: https://sid.ir/paper/1065507/en

IEEE: Copy

SAYED RASUL SHAFE MEHRABADI, BAHAREH SADEGHI, Mohammad Hossein Mosslemin, and Saeedeh Hashemian, “Nano-cellulose-OSnCl4-x: Green and natural-based renewable nanocatalyst for one-pot synthesis of 2-amino-3-phenylsulfonyl-4H-pyran derivatives,” IRANIAN JOURNAL OF CATALYSIS, vol. 12, no. 4, pp. 407–416, 2022, [Online]. Available: https://sid.ir/paper/1065507/en

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