Synthesis and Evaluation of Nano Zeolite Na/Al as a New Modifier for Electrochemical Determination of Acetaminophen

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Arabi Afroozeh; Mohadesi Alireza; Karimi Mohammad Ali; Ranjbar Mehdi

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Journal Paper

Paper Information

Journal: Iranian Journal of Analytical Chemistry Year:2022 | Volume:9 | Issue:1 Page(s): 88-96

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Information Journal Paper

Title

Synthesis and Evaluation of Nano Zeolite Na/Al as a New Modifier for Electrochemical Determination of Acetaminophen

Author(s)

Arabi Afroozeh | Mohadesi Alireza | Karimi Mohammad Ali | Ranjbar Mehdi | Issue Writer Certificate

Keywords

Zeolite Al/NaQ4

Carbon Paste ElectrodeQ4

AcetaminophenQ4

ElectroanalysisQ4

Abstract

In this study, a new Zeolite Al/Na (ZAN) was synthesized and characterized and then a new modified Carbon Paste Electrode with ZAN was made to determine Acetaminophen. Electrochemical studies using Linear Sweep Voltammetry and differential pulse voltammetry were used to determine electrochemical Acetaminophen . In the presence of Acetaminophen , modified electrode with ZAN shows a specific anodic peak at ~ 0.59 volts which is the result of using electrocatalytic oxidation of Acetaminophen . The determination limit of this method to measure Acetaminophen was 5.8 µM, the relative standard deviation for 7 repeated measurements was 1.1 % and linear range of the calibration to measure Acetaminophen was 10 up to 115 µM . for the characterization of ZAN nanostructures we used SEM (Scanning Electron Microscopy), DLS (Dynamic Light Scattering) and FT-IR (Fourier-Transform Infrared spectroscopy).

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