Organo-Clay Composites of Intercalated 4-Methylaniline and Its Schiff Base Derivative: Preparation and Characterization

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Al Sarray Ali Jabbar; Al Mussawi Israa M.; Al Noor Taghreed H.; Abu Zaid Yousif

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Journal Paper

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Journal: Journal of Medicinal and Chemical Sciences Year:621 | Volume: | Issue: Page(s): 1094-1101

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Title

Organo-Clay Composites of Intercalated 4-Methylaniline and Its Schiff Base Derivative: Preparation and Characterization

Author(s)

Al Sarray Ali Jabbar | Al Mussawi Israa M. | Al Noor Taghreed H. | Abu Zaid Yousif | Issue Writer Certificate

Keywords

Schiff baseQ4

p-toluidineQ4

BentoniteQ4

IntercalationQ4

organo-clay compositeQ4

Abstract

4-methylaniline and its Schiff base derivative were intercalated into the Bentonite clay interlayers in a solid state reaction followed by a condensation reaction to produce two organo-clay composites. X-ray diffraction was used to identify the changes in basal spacing of montmorillonite layers which exhibited noticeable alteration before and after the formation of the composites. FT-IR spectra, on the other hand, were utilized for identifying the structural compositions of the prepared materials as well as the formation of the intercalated Schiff base derivative. The surface morphology of the composites was examined by Scanning Electron Microscopy SEM and Atomic Force Microscope AFM, which reflected some differences in the surface of prepared composites as the particle size decreased with the Schiff base formation.

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