EFFECT OF PH ON PRODUCTION PROCESS AND CHARACTERISTICS OF ZIRCONIUM CARBIDE NANO PARTICLES SYNTHESIZED BY SOL-GEL METHOD

Q: How can I download an article?

To download an article from SID, first log in to the site, search for the article title, and click on the 'Download Article' option.

Q: How can I download an ISI article?

To download an ISI article on SID, enter the keyword or article title in the search bar, view the relevant results, click on the desired article, and select the 'Download Article' option.

Q: How can I access the SID database?

To access the SID database, visit SID.ir, create an account, and log in to access scientific resources.

Q: Is downloading articles from SID free?

Some articles on SID are available for free, while others require payment. Details are specified on the article's page.

SHAYESTEFAR M.; BAGHSHAHI S.; MIRHADI B.

Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

Paper Information

Journal: JOURNAL OF NEW MATERIALS Year:2016 | Volume:7 | Issue:1 Page(s): 1-12

Download Full-Text

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Persian Verion

View:

1,169

Download:

Cites:

Information Journal Paper

Title

EFFECT OF PH ON PRODUCTION PROCESS AND CHARACTERISTICS OF ZIRCONIUM CARBIDE NANO PARTICLES SYNTHESIZED BY SOL-GEL METHOD

Author(s)

SHAYESTEFAR M. | BAGHSHAHI S. | MIRHADI B. | Issue Writer Certificate

Keywords

SOLQ2

GELQ2

NANO PARTICLEQ1

ZIRCONIUM CARBIDEQ1

PARTICLES SIZEQ2

Abstract

Zirconium carbide NANO PARTICLE was synthesized through SOL-gel method. Although SOL-gel process is usually used to producing oxide compounds, in this study it was successfully employed to produce a carbide powder. For this purpose, zirconium propoxide and saccharose were initially used as zirconium and carbon sources, respectively. The starting SOL was produced in 5 different pH, in order to examine its effects on the properties of the obtained powder. Heat-treatment of the GEL, in a range of 700-1400 °C, resulted in the formation of mixed zirconia-carbon powder, and subsequently, ZIRCONIUM CARBIDE. Then, differential thermal analysis (DTA), X-ray diffraction (XRD) and scanning electron microscopy (SEM) were used to investigate heat performance of the GEL, structure and micro-structures of the synthesized powder, respectively. Results showed that increasing the pH could not only affect the reaction process and efficiency of the ZIRCONIUM CARBIDE synthesis, but it also decreased the PARTICLES SIZE of the powder. Therefore, at pH 4.2, 5.2 and 6.2, the size ranges of 130-190, 90-150 and 50-100 nm were obtained, respectively. It was also noted that changes in pH had no effects on the morphology of the spherical particles.

Cites

No record.

References

No record.

Cite

APA: Copy

SHAYESTEFAR, M., BAGHSHAHI, S., & MIRHADI, B.. (2016). EFFECT OF PH ON PRODUCTION PROCESS AND CHARACTERISTICS OF ZIRCONIUM CARBIDE NANO PARTICLES SYNTHESIZED BY SOL-GEL METHOD. JOURNAL OF NEW MATERIALS, 7(1), 1-12. SID. https://sid.ir/paper/169745/en

Vancouver: Copy

SHAYESTEFAR M., BAGHSHAHI S., MIRHADI B.. EFFECT OF PH ON PRODUCTION PROCESS AND CHARACTERISTICS OF ZIRCONIUM CARBIDE NANO PARTICLES SYNTHESIZED BY SOL-GEL METHOD. JOURNAL OF NEW MATERIALS[Internet]. 2016;7(1):1-12. Available from: https://sid.ir/paper/169745/en

IEEE: Copy

M. SHAYESTEFAR, S. BAGHSHAHI, and B. MIRHADI, “EFFECT OF PH ON PRODUCTION PROCESS AND CHARACTERISTICS OF ZIRCONIUM CARBIDE NANO PARTICLES SYNTHESIZED BY SOL-GEL METHOD,” JOURNAL OF NEW MATERIALS, vol. 7, no. 1, pp. 1–12, 2016, [Online]. Available: https://sid.ir/paper/169745/en

Related Journal Papers