MECHANOCHEMICAL SYNTHESIS OF NANO-STRUCTURED MOLYBDENUM CARBIDE WITH MOS2/CAO/C SYSTEM IN THE PRESENCE OF ALUMINUM POWDER

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FEKRI N.; VAHDATI KHAKI J.; ALAEI M.; RASHIDI A.M.; VARAMESH A.

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Journal: Journal of Applied Research in Chemistry Year:2012 | Volume:6 | Issue:2 Page(s): 57-67

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Title

MECHANOCHEMICAL SYNTHESIS OF NANO-STRUCTURED MOLYBDENUM CARBIDE WITH MOS2/CAO/C SYSTEM IN THE PRESENCE OF ALUMINUM POWDER

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Keywords

MECHANOCHEMICAL SYNTHESISQ2

NANOSTRUCTURE MO2CQ2

CATALYSTQ2

Abstract

We have been successfully prepared molybdenum carbide nanostructures by mechanochemical method from molybdenite in the presence of aluminum powder, lime and carbon. The heat released from aluminothermy reaction assisted the reaction progress. Therefore, the reaction was performed in the presence of aluminum powder.The reaction was done without heating, and the sulfur that released during reaction progress was removed as calcium sulfide that was a solid composition without any environmental pollution.Various parameters such as milling time and different amounts of aluminum powder have been considered to achieve optimum conditions.The as-prepared samples were identified with X-ray diffraction (XRD) and scanning electron microscopy (SEM).

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APA: Copy

FEKRI, N., VAHDATI KHAKI, J., ALAEI, M., RASHIDI, A.M., & VARAMESH, A.. (2012). MECHANOCHEMICAL SYNTHESIS OF NANO-STRUCTURED MOLYBDENUM CARBIDE WITH MOS₂/CAO/C SYSTEM IN THE PRESENCE OF ALUMINUM POWDER. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), 6(2), 57-67. SID. https://sid.ir/paper/179978/en

Vancouver: Copy

FEKRI N., VAHDATI KHAKI J., ALAEI M., RASHIDI A.M., VARAMESH A.. MECHANOCHEMICAL SYNTHESIS OF NANO-STRUCTURED MOLYBDENUM CARBIDE WITH MOS₂/CAO/C SYSTEM IN THE PRESENCE OF ALUMINUM POWDER. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC)[Internet]. 2012;6(2):57-67. Available from: https://sid.ir/paper/179978/en

IEEE: Copy

N. FEKRI, J. VAHDATI KHAKI, M. ALAEI, A.M. RASHIDI, and A. VARAMESH, “MECHANOCHEMICAL SYNTHESIS OF NANO-STRUCTURED MOLYBDENUM CARBIDE WITH MOS₂/CAO/C SYSTEM IN THE PRESENCE OF ALUMINUM POWDER,” JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), vol. 6, no. 2, pp. 57–67, 2012, [Online]. Available: https://sid.ir/paper/179978/en

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