SYNTHESIS OF ZRO2 ON Y-AL2O3 NANOCATALYST BY REVERSE MICROEMULSION METHOD FOR ETHANOL AUTO-THERMAL REFORMING PROCESS

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LOTFI R.; ABEDINI KHORRAMI S.; MOTIEE F.; MORADI DEHAGHI SH.; DERAKHSHI P.

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Journal: Journal of Applied Research in Chemistry Year:2016 | Volume:10 | Issue:2 Page(s): 43-52

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Title

SYNTHESIS OF ZRO2 ON Y-AL2O3 NANOCATALYST BY REVERSE MICROEMULSION METHOD FOR ETHANOL AUTO-THERMAL REFORMING PROCESS

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Keywords

AUTO-THERMAL REFORMINGQ2

HYDROGEN PRODUCTIONQ1

FIXED BED REACTORQ2

ALUMINUM OXIDEQ2

ZIRCONIUM OXIDEQ2

Abstract

The present work focused on the investigation of hydrogen generation through the ethanol AUTO-THERMAL REFORMING (ATR) with ZrO2 over gama ALUMINUM OXIDE catalysts. Monodispered colloidal ZIRCONIUM OXIDE was synthesized by water-in-oil microemulsion using ZrOCl2.8H2O and NH4OH. ZrO2/g-Al2O3 catalysts were prepared by dispersing highly stable ZrO2 nanoparticles on γ-Alumina by mechanical stirring. The effect of the particle size was studied by varying the molar ratio of Zr: Al. Catalysts were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray diffraction (XRD) techniques. The results obtained from temperature programmed reduction (TPR) technique, confirmed the uniformity of ZrO2 dispersion over the carrier. The particle size were distributed in 12-27 nm range. Also, in this research, AUTO-THERMAL REFORMING of ethanol was conducted in a quartz FIXED BED REACTOR at atmospheric pressure. The exiting gases of the reactor were analyzed with on line gas chromatography. Among the catalysts tested, Zr: Al (1.0: 3.0) molar ratio showed to be the best catalytic performance in HYDROGEN PRODUCTION by ATR.

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APA: Copy

LOTFI, R., ABEDINI KHORRAMI, S., MOTIEE, F., MORADI DEHAGHI, SH., & DERAKHSHI, P.. (2016). SYNTHESIS OF ZRO₂ ON Y-AL₂O₃ NANOCATALYST BY REVERSE MICROEMULSION METHOD FOR ETHANOL AUTO-THERMAL REFORMING PROCESS. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), 10(2), 43-52. SID. https://sid.ir/paper/180020/en

Vancouver: Copy

LOTFI R., ABEDINI KHORRAMI S., MOTIEE F., MORADI DEHAGHI SH., DERAKHSHI P.. SYNTHESIS OF ZRO₂ ON Y-AL₂O₃ NANOCATALYST BY REVERSE MICROEMULSION METHOD FOR ETHANOL AUTO-THERMAL REFORMING PROCESS. JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC)[Internet]. 2016;10(2):43-52. Available from: https://sid.ir/paper/180020/en

IEEE: Copy

R. LOTFI, S. ABEDINI KHORRAMI, F. MOTIEE, SH. MORADI DEHAGHI, and P. DERAKHSHI, “SYNTHESIS OF ZRO₂ ON Y-AL₂O₃ NANOCATALYST BY REVERSE MICROEMULSION METHOD FOR ETHANOL AUTO-THERMAL REFORMING PROCESS,” JOURNAL OF APPLIED RESEARCHES IN CHEMISTRY (JARC), vol. 10, no. 2, pp. 43–52, 2016, [Online]. Available: https://sid.ir/paper/180020/en

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