OPTIMIZED CONDITIONS FOR PURIFICATION OF DMAZ VIA VACUUM DISTILLATION IN LAB SCALE

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GHANBARI PAKDEHI S.; ROUHANDEH H.; SANAEI H.R.; KHODAYEE M.

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Journal: TAHGHIGH VA TOWSE MAVAD POR ENERGY Year:2012 | Volume:7 | Issue:3 (15) Page(s): 37-44

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Title

OPTIMIZED CONDITIONS FOR PURIFICATION OF DMAZ VIA VACUUM DISTILLATION IN LAB SCALE

Author(s)

GHANBARI PAKDEHI S. | ROUHANDEH H. | SANAEI H.R. | KHODAYEE M. | Issue Writer Certificate

Keywords

DMAZQ3

PURIFICATIONQ3

VACUUM DISTILLATIONQ3

OPTIMIZATIONQ2

Abstract

Dimethyl amino ethane azide (DMAZ) is a good replacement of hydrazine derivatives in aerospace industries. It is produced from the reaction between dimethyl amino ethyl chloride and aqueous sodium azide. DMAZ is formed in organic phase with a purity of at least 90%. High pure DMAZ is necessary for aerospace utilization. Thermal sensitivity of DMAZ leads the PURIFICATION procedure to be performed at low temperatures. So, the Distillation at sub-atmospheric pressures is a good choice for this purpose. In this paper, effect of various parameters such as temperature and pressure on the distillation time and loss of material and final purity of DMAZ was studied in regular packed column, known as vigorous column, and optimized conditions were found.

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APA: Copy

GHANBARI PAKDEHI, S., ROUHANDEH, H., SANAEI, H.R., & KHODAYEE, M.. (2012). OPTIMIZED CONDITIONS FOR PURIFICATION OF DMAZ VIA VACUUM DISTILLATION IN LAB SCALE. TAHGHIGH VA TOWSE MAVAD POR ENERGY, 7(3 (15)), 37-44. SID. https://sid.ir/paper/211754/en

Vancouver: Copy

GHANBARI PAKDEHI S., ROUHANDEH H., SANAEI H.R., KHODAYEE M.. OPTIMIZED CONDITIONS FOR PURIFICATION OF DMAZ VIA VACUUM DISTILLATION IN LAB SCALE. TAHGHIGH VA TOWSE MAVAD POR ENERGY[Internet]. 2012;7(3 (15)):37-44. Available from: https://sid.ir/paper/211754/en

IEEE: Copy

S. GHANBARI PAKDEHI, H. ROUHANDEH, H.R. SANAEI, and M. KHODAYEE, “OPTIMIZED CONDITIONS FOR PURIFICATION OF DMAZ VIA VACUUM DISTILLATION IN LAB SCALE,” TAHGHIGH VA TOWSE MAVAD POR ENERGY, vol. 7, no. 3 (15), pp. 37–44, 2012, [Online]. Available: https://sid.ir/paper/211754/en

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