SYNTHESIS OF 4-TERTIARBUTYL CATECHOL (TBC) USING ION EXCHANGE RESIN AS A CATALYST

Q: How can I download an article?

To download an article from SID, first log in to the site, search for the article title, and click on the 'Download Article' option.

Q: How can I download an ISI article?

To download an ISI article on SID, enter the keyword or article title in the search bar, view the relevant results, click on the desired article, and select the 'Download Article' option.

Q: How can I access the SID database?

To access the SID database, visit SID.ir, create an account, and log in to access scientific resources.

Q: Is downloading articles from SID free?

Some articles on SID are available for free, while others require payment. Details are specified on the article's page.

MASIHI SHABRONIAN J.; SOLEYMANI JAMARANI M.; HAJI ALI AKBARI F.

مرکز اطلاعات علمی Scientific Information Database (SID) - Trusted Source for Research and Academic Resources

Journal Paper

Paper Information

Journal: JOURNAL OF SCIENCE (UNIVERSITY OF TEHRAN) (JSUT) Year:2007 | Volume:33 | Issue:2 (SECTION: CHEMISTRY) Page(s): 9-13

Download Full-Text

Persian Verion

View:

2,753

Download:

Cites:

Information Journal Paper

Title

SYNTHESIS OF 4-TERTIARBUTYL CATECHOL (TBC) USING ION EXCHANGE RESIN AS A CATALYST

Author(s)

MASIHI SHABRONIAN J. | SOLEYMANI JAMARANI M. | HAJI ALI AKBARI F. | Issue Writer Certificate

Keywords

ANTIOXIDANTQ3

TBCQ3

TERTIARY BUTHYL CATECHOLQ3

ALKYLATIONQ3

CATECHOLQ3

PYROCATECHOLQ3

Abstract

4- Tertiarybutyl CATECHOL (TBC) is classified as a two-valance phenolic ANTIOXIDANT, which can be used in greases, industrial oils, and polyurethanes as polymerization inhibitor and thermal stablizer. This compound scavenges radicals and prevents the chain reaction from proceeding. Also this compound is used in BD (butadiene) unit as an ANTIOXIDANT. In this paper we report a practical procedure for the synthesis of TBC using CATECHOL and isobutylene in the presence of an ion exchange resin as a catalyst in good yield. Important parameters in the reaction are catalyst, temperature, and reaction time and flow gas. The reaction and product formation are monitored by thin layer chromatography, gas chromatography (GC), FT-IR and FT-HNMR spectroscopy. Reaction yield is 84.9% and products purity after distillation at low pressure above 95% and greater than purity of available standard TBC that equals to 95%. This purity is high enough for industrial application of TBC.

Cites

No record.

References

No record.

Cite

APA: Copy

MASIHI SHABRONIAN, J., SOLEYMANI JAMARANI, M., & HAJI ALI AKBARI, F.. (2007). SYNTHESIS OF 4-TERTIARBUTYL CATECHOL (TBC) USING ION EXCHANGE RESIN AS A CATALYST. JOURNAL OF SCIENCE (UNIVERSITY OF TEHRAN) (JSUT), 33(2 (SECTION: CHEMISTRY)), 9-13. SID. https://sid.ir/paper/2192/en

Vancouver: Copy

MASIHI SHABRONIAN J., SOLEYMANI JAMARANI M., HAJI ALI AKBARI F.. SYNTHESIS OF 4-TERTIARBUTYL CATECHOL (TBC) USING ION EXCHANGE RESIN AS A CATALYST. JOURNAL OF SCIENCE (UNIVERSITY OF TEHRAN) (JSUT)[Internet]. 2007;33(2 (SECTION: CHEMISTRY)):9-13. Available from: https://sid.ir/paper/2192/en

IEEE: Copy

J. MASIHI SHABRONIAN, M. SOLEYMANI JAMARANI, and F. HAJI ALI AKBARI, “SYNTHESIS OF 4-TERTIARBUTYL CATECHOL (TBC) USING ION EXCHANGE RESIN AS A CATALYST,” JOURNAL OF SCIENCE (UNIVERSITY OF TEHRAN) (JSUT), vol. 33, no. 2 (SECTION: CHEMISTRY), pp. 9–13, 2007, [Online]. Available: https://sid.ir/paper/2192/en

Related Journal Papers