SYNTHESIS OF CELLULOSE BASED GRAFT POLYMERS USING METAL-CATALYZED LIVING RADICAL POLYMERIZATION

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ABBASIYAN M.; PAKZAD M.

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Journal: JOURNAL OF APPLIED CHEMISTRY Year:2016 | Volume:11 | Issue:39 Page(s): 85-98

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Title

SYNTHESIS OF CELLULOSE BASED GRAFT POLYMERS USING METAL-CATALYZED LIVING RADICAL POLYMERIZATION

Author(s)

ABBASIYAN M. | PAKZAD M. | Issue Writer Certificate

Keywords

CELLULOSEQ2

ATRPQ2

ACRYLONITRILEQ2

STYRENEQ2

GRAFT COPOLYMERQ1

Abstract

A copolymer composed of STYRENE and ACRYLONITRILE was grafted onto CELLULOSE backbone by free radical polymerization and atom transfer radical polymerization (ATRP) method. First, STYRENE was grafted onto CELLULOSE Fibers by using suspension polymerization and free-radical polymerization technique. Potassium persulfate (PPS) was used as a chemical initiator and water was used as a medium. We used CELLULOSE-graft-polystyrene as a starting polymer and N-bromosuccinimide (NBS) as a brominating agent to obtain polymers with bromine group. This brominated CELLULOSE fibers were used as an ATRP macroinitiator. This macroinitiator can polymerize ACRYLONITRILE in the presence of CuCl / 2, 2'-Bipyridine (Bpy) catalyst system, in THF solvent at 90oC. The formation of the GRAFT COPOLYMER was confirmed with FTIR, XRD, SEM, TGA and DSC methods.

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APA: Copy

ABBASIYAN, M., & PAKZAD, M.. (2016). SYNTHESIS OF CELLULOSE BASED GRAFT POLYMERS USING METAL-CATALYZED LIVING RADICAL POLYMERIZATION. JOURNAL OF APPLIED CHEMISTRY, 11(39), 85-98. SID. https://sid.ir/paper/243313/en

Vancouver: Copy

ABBASIYAN M., PAKZAD M.. SYNTHESIS OF CELLULOSE BASED GRAFT POLYMERS USING METAL-CATALYZED LIVING RADICAL POLYMERIZATION. JOURNAL OF APPLIED CHEMISTRY[Internet]. 2016;11(39):85-98. Available from: https://sid.ir/paper/243313/en

IEEE: Copy

M. ABBASIYAN, and M. PAKZAD, “SYNTHESIS OF CELLULOSE BASED GRAFT POLYMERS USING METAL-CATALYZED LIVING RADICAL POLYMERIZATION,” JOURNAL OF APPLIED CHEMISTRY, vol. 11, no. 39, pp. 85–98, 2016, [Online]. Available: https://sid.ir/paper/243313/en

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