Investigation of Cooling Crystallization Parameters on the Morphologic Properties of Ammonium Perchlorate Crystals by Taguchi Method

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Hosseini Seyed Ghorban; Kashi Abolfazl; Bazrafshan Esmaeil

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Paper Information

Journal: Nashrieh Shimi va Mohandesi Shimi Iran Year:2019 | Volume:37 | Issue:4 (90) Page(s): 223-233

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Information Journal Paper

Title

Investigation of Cooling Crystallization Parameters on the Morphologic Properties of Ammonium Perchlorate Crystals by Taguchi Method

Author(s)

Hosseini Seyed Ghorban | Kashi Abolfazl | Bazrafshan Esmaeil | Issue Writer Certificate

Keywords

Cooling crystallizationQ1

Ammonium perchlorateQ1

MorphologyQ2

Taguchi’Q2

s methodQ1

Scanning Electron mMicroscopy (SEM)Q1

Abstract

This research is aimed to investigate the effect of crystallization parameters like cooling rate, seeding ratio, a cooling trend, and agitation intensity on the morphological properties of Ammonium perchlorate crystals. A solution of AP was prepared by solving industrial grade Ammonium perchlorate into the pure water and recrystallization was conducted using a 1. 3 L agitated batch crystallizer. The effects of the selected parameters were analyzed by applying Taguchi’; s method. Resulted crystals were characterized by X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM). The results indicate that the cooling rate has the greatest contribution to the roundness of the crystals and by optimization of the parameters, roundness and its standard deviation have been improved by 9. 4% and 79% respectively. Compared to the industrial crystals, the crystallinity of the resulted crystals was also substantially enhanced.

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APA: Copy

Hosseini, Seyed Ghorban, Kashi, Abolfazl, & Bazrafshan, Esmaeil. (2019). Investigation of Cooling Crystallization Parameters on the Morphologic Properties of Ammonium Perchlorate Crystals by Taguchi Method. NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN), 37(4 (90) ), 223-233. SID. https://sid.ir/paper/26037/en

Vancouver: Copy

Hosseini Seyed Ghorban, Kashi Abolfazl, Bazrafshan Esmaeil. Investigation of Cooling Crystallization Parameters on the Morphologic Properties of Ammonium Perchlorate Crystals by Taguchi Method. NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN)[Internet]. 2019;37(4 (90) ):223-233. Available from: https://sid.ir/paper/26037/en

IEEE: Copy

Seyed Ghorban Hosseini, Abolfazl Kashi, and Esmaeil Bazrafshan, “Investigation of Cooling Crystallization Parameters on the Morphologic Properties of Ammonium Perchlorate Crystals by Taguchi Method,” NASHRIEH SHIMI VA MOHANDESI SHIMI IRAN (PERSIAN), vol. 37, no. 4 (90) , pp. 223–233, 2019, [Online]. Available: https://sid.ir/paper/26037/en

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