SYNTHESIS OF MGAL2O4-TI(C,N) NANOCOMPOSITE BY ALUMINOTHERMIC REDUCTION

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KHOSHOMID AGHDAM E.; NAGHIZADEH R.; REZAIE H.R.

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Journal Paper

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Journal: Iranian Journal of Materials Science and Engineering Year:2015 | Volume:12 | Issue:3 Page(s): 75-82

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Title

SYNTHESIS OF MGAL2O4-TI(C,N) NANOCOMPOSITE BY ALUMINOTHERMIC REDUCTION

Author(s)

KHOSHOMID AGHDAM E. | NAGHIZADEH R. | REZAIE H.R. | Issue Writer Certificate

Keywords

MGAL2O4-TI(C

N) COMPOSITE

ALUMINOTHERMIC REACTION

COKE BED

TIC

TIN

SPINEL

Abstract

MgAl2O4/Ti(C,N) composites were synthesized through aluminothermic reaction between Al,TiO2,MgO powders and phenolic resin in coke bed condition. Effect of addition of carbon black and sugar into the mixture at different temperatures were investigated. The phases and microstructures of samples were investigated by X-ray diffraction (XRD) and scanning electron microscopy (SEM). MgAl2O4/Ti(C,N) composites without additive were obtained after heat treatment at 1600 oC. With addition of carbon black TiC, TiN and Ti(C,N) were appeared after firing at 1400 °C and formation of spinel/Ti(C,N) composites were completed at 1600°C. In sample containing sugar, MgAl2O4-Ti(C,N) composite were completely synthesized at 1400 °C. In this sample crystallite size of Ti(C,N) were 32 nm and carbon content of titanium carbonitride (Ti(C,N)) reached to 0.442 value.

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APA: Copy

KHOSHOMID AGHDAM, E., NAGHIZADEH, R., & REZAIE, H.R.. (2015). SYNTHESIS OF MGAL₂O₄-TI(C,N) NANOCOMPOSITE BY ALUMINOTHERMIC REDUCTION. IRANIAN JOURNAL OF MATERIALS SCIENCE AND ENGINEERING, 12(3), 75-82. SID. https://sid.ir/paper/276824/en

Vancouver: Copy

KHOSHOMID AGHDAM E., NAGHIZADEH R., REZAIE H.R.. SYNTHESIS OF MGAL₂O₄-TI(C,N) NANOCOMPOSITE BY ALUMINOTHERMIC REDUCTION. IRANIAN JOURNAL OF MATERIALS SCIENCE AND ENGINEERING[Internet]. 2015;12(3):75-82. Available from: https://sid.ir/paper/276824/en

IEEE: Copy

E. KHOSHOMID AGHDAM, R. NAGHIZADEH, and H.R. REZAIE, “SYNTHESIS OF MGAL₂O₄-TI(C,N) NANOCOMPOSITE BY ALUMINOTHERMIC REDUCTION,” IRANIAN JOURNAL OF MATERIALS SCIENCE AND ENGINEERING, vol. 12, no. 3, pp. 75–82, 2015, [Online]. Available: https://sid.ir/paper/276824/en

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