SYNTHESIS, SPECTROSCOPIC, THERMAL, CRYSTAL CHARACTERIZATION AND BIOLOGICAL ACTIVITY OF {[NI(PHEN)3][NI(DIPIC)2]}2.17H2O (H2DIPIC: PYRIDINE-2,6-DICARBOXYLIC ACID, PHEN: 1,10-PHENANTHROLINE)

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COLAK A.T.; COLAK F.; YESILEL O.Z.; SAHIN E.

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Paper Information

Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2010 | Volume:7 | Issue:2 Page(s): 384-393

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Title

SYNTHESIS, SPECTROSCOPIC, THERMAL, CRYSTAL CHARACTERIZATION AND BIOLOGICAL ACTIVITY OF {[NI(PHEN)3][NI(DIPIC)2]}2.17H2O (H2DIPIC: PYRIDINE-2,6-DICARBOXYLIC ACID, PHEN: 1,10-PHENANTHROLINE)

Author(s)

COLAK A.T. | COLAK F. | YESILEL O.Z. | SAHIN E. | Issue Writer Certificate

Keywords

DIPICOLINATO COMPLEX

10-PHENANTHROLINE COMPLEX

NICKEL (II) COMPLEX

ANTIMICROBIAL ACTIVITY

Abstract

The new {[Ni(phen)3][Ni(dipic)2]}2.17H2O (1) (phen=1,10-phenanthroline, dipic=dipicolinate)) has been prepared and characterized by elemental analysis, IR, UV-Vis, magnetic measurement and single crystal X-ray diffraction. The complex consists of two tris (1,10-phenanthroline) nickel (II) cations, two bis (dipicolinato)nickelate (II) anions and seventeen uncoordinated water molecules. The Ni (II) complex crystallizes in the triclinic space group P-1. The complex consisting of cation has distorted octahedral coordination by three bidentate phen ligands. In the complex anion, each dipic ligand simultaneously exhibits tridentate coordination modes through N atom of pyridine ring and oxygen atoms of the carboxylate groups. The crystal packing of 1 is a composite of intermolecular hydrogen bonding, π-π and C-H...π interactions. The complex has also been investigated in terms of biological activity and it showed high activity against S. aureus fromGram positive bacteria and C. albicans from yeast tested.

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APA: Copy

COLAK, A.T., COLAK, F., YESILEL, O.Z., & SAHIN, E.. (2010). SYNTHESIS, SPECTROSCOPIC, THERMAL, CRYSTAL CHARACTERIZATION AND BIOLOGICAL ACTIVITY OF {[NI(PHEN)₃][NI(DIPIC)₂]}₂.17H₂O (H₂DIPIC: PYRIDINE-2,6-DICARBOXYLIC ACID, PHEN: 1,10-PHENANTHROLINE). JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 7(2), 384-393. SID. https://sid.ir/paper/282381/en

Vancouver: Copy

COLAK A.T., COLAK F., YESILEL O.Z., SAHIN E.. SYNTHESIS, SPECTROSCOPIC, THERMAL, CRYSTAL CHARACTERIZATION AND BIOLOGICAL ACTIVITY OF {[NI(PHEN)₃][NI(DIPIC)₂]}₂.17H₂O (H₂DIPIC: PYRIDINE-2,6-DICARBOXYLIC ACID, PHEN: 1,10-PHENANTHROLINE). JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2010;7(2):384-393. Available from: https://sid.ir/paper/282381/en

IEEE: Copy

A.T. COLAK, F. COLAK, O.Z. YESILEL, and E. SAHIN, “SYNTHESIS, SPECTROSCOPIC, THERMAL, CRYSTAL CHARACTERIZATION AND BIOLOGICAL ACTIVITY OF {[NI(PHEN)₃][NI(DIPIC)₂]}₂.17H₂O (H₂DIPIC: PYRIDINE-2,6-DICARBOXYLIC ACID, PHEN: 1,10-PHENANTHROLINE),” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 7, no. 2, pp. 384–393, 2010, [Online]. Available: https://sid.ir/paper/282381/en

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