SYNTHESIS, SPECTROSCOPIC AND ELECTROCHEMICAL CHARACTERISTICS OF A NOVEL SCHIFF-BASE FROM SACCHARIN AND TRYPTOPHAN

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CAKIR S.; BICER E.

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ISSN: 2588-4824

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2010 | Volume:7 | Issue:2 Page(s): 394-404

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Title

SYNTHESIS, SPECTROSCOPIC AND ELECTROCHEMICAL CHARACTERISTICS OF A NOVEL SCHIFF-BASE FROM SACCHARIN AND TRYPTOPHAN

Author(s)

CAKIR S. | BICER E. | Issue Writer Certificate

Keywords

SCHIFF-BASE

TRYPTOPHAN

SACCHARIN

VOLTAMMETRY

SPECTROSCOPY

Abstract

In the present work, a novel SCHIFF-BASE was synthesized by the reaction of SACCHARIN with TRYPTOPHAN and characterized by elemental analysis as well as UV-Vis, FT-IR, 1H NMR spectroscopic data. The voltammetric behavior of SCHIFF-BASE was also studied on the hanging mercury drop electrode (HMDE) by using Square-Wave VOLTAMMETRY (SWV) and Cyclic VOLTAMMETRY (CV) techniques. The voltammograms of the SCHIFF-BASE exhibited two irreversible reduction peaks in Britton-Robinson buffer (pH 7.0-10.0) for the potential range from 0.0 V to -1.4 V. These peaks which appeared at more positive potentials than the reduction peaks of TRYPTOPHAN and SACCHARIN, may be assigned to the cathodic reductions of C-N+ and >C=N- moieties of SCHIFF-BASE.

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APA: Copy

CAKIR, S., & BICER, E.. (2010). SYNTHESIS, SPECTROSCOPIC AND ELECTROCHEMICAL CHARACTERISTICS OF A NOVEL SCHIFF-BASE FROM SACCHARIN AND TRYPTOPHAN. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 7(2), 394-404. SID. https://sid.ir/paper/282382/en

Vancouver: Copy

CAKIR S., BICER E.. SYNTHESIS, SPECTROSCOPIC AND ELECTROCHEMICAL CHARACTERISTICS OF A NOVEL SCHIFF-BASE FROM SACCHARIN AND TRYPTOPHAN. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2010;7(2):394-404. Available from: https://sid.ir/paper/282382/en

IEEE: Copy

S. CAKIR, and E. BICER, “SYNTHESIS, SPECTROSCOPIC AND ELECTROCHEMICAL CHARACTERISTICS OF A NOVEL SCHIFF-BASE FROM SACCHARIN AND TRYPTOPHAN,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 7, no. 2, pp. 394–404, 2010, [Online]. Available: https://sid.ir/paper/282382/en

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