SYNTHESIS AND CHARACTERIZATION OF 2-ALKYL -5-{4-[(3-NITROPHENYL-5-ISOXAZOLYL)METHOXY]PHENYL}-2H-TETRAZOLES

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MIRZAEI Y.R.; EJLALI L.

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ISSN: 2588-4824

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Journal: JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS) Year:2010 | Volume:7 | Issue:3 Page(s): 685-694

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Title

SYNTHESIS AND CHARACTERIZATION OF 2-ALKYL -5-{4-[(3-NITROPHENYL-5-ISOXAZOLYL)METHOXY]PHENYL}-2H-TETRAZOLES

Author(s)

MIRZAEI Y.R. | EJLALI L. | Issue Writer Certificate

Keywords

ISOXAZOLYL-TETRAZOLYL ETHERS

[3+2] CYCLOADDITION

ISOXAZOLE

NITRO COMPOUNDS

TETRAZOLE

Abstract

Heteroaryl substituted analogs of antirhnoviral (A), was prepared by a convergent approach. 3-Nitrophenyl-5- bromooromethylisoxazoles 5a-b were synthesized by [3+2] cycloaddition of 3-(benzoyloxy)-propyne 2 to in situ generated arylnitrile oxides followed by deprotection of cycloadducts 3a-b and bromination of the resulting alcohols 4a-b. Coupling of 3- nitrophenyl-5-bromooromethylisoxazoles (5a-b) with 4-[5-(2-alkyl-2H-tetrazolyl)]phenols (6a-d) in N-methylpyrrolidinone under mild conditions afforded a new series of 2-alkyl-5-{4-[1-(3-nitrophenyl-5-isoxazolyl)methyloxy]phenyl}-2H-tetrazoles (7a-h) in high yields. The structures of the synthesized compounds were confirmed by their 1H NMR, Mass spectral, and Elemental Analysis data.

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APA: Copy

MIRZAEI, Y.R., & EJLALI, L.. (2010). SYNTHESIS AND CHARACTERIZATION OF 2-ALKYL -5-{4-[(3-NITROPHENYL-5-ISOXAZOLYL)METHOXY]PHENYL}-2H-TETRAZOLES. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), 7(3), 685-694. SID. https://sid.ir/paper/282465/en

Vancouver: Copy

MIRZAEI Y.R., EJLALI L.. SYNTHESIS AND CHARACTERIZATION OF 2-ALKYL -5-{4-[(3-NITROPHENYL-5-ISOXAZOLYL)METHOXY]PHENYL}-2H-TETRAZOLES. JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS)[Internet]. 2010;7(3):685-694. Available from: https://sid.ir/paper/282465/en

IEEE: Copy

Y.R. MIRZAEI, and L. EJLALI, “SYNTHESIS AND CHARACTERIZATION OF 2-ALKYL -5-{4-[(3-NITROPHENYL-5-ISOXAZOLYL)METHOXY]PHENYL}-2H-TETRAZOLES,” JOURNAL OF THE IRANIAN CHEMICAL SOCIETY(JICS), vol. 7, no. 3, pp. 685–694, 2010, [Online]. Available: https://sid.ir/paper/282465/en

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